An Experimental Study of Crystal Size Distribution in a Continuous, Backmixed, Gas-Phase Reactor

  • Paul D. Stone
  • Alan D. Randolph


One of the most important aspects of a process producing a solid-phase product is the particle size distribution obtained in the process. Although much has been done on liquid-phase crystallization, and on single crystal growth from the gaseous phase, little work has been reported in the area of particle size distributions from a continuous, gas-phase process. Discussed in this paper will be the efforts of the authors in designing and utilizing a single-stage, backmixed reactor to study crystal size distribution (CSD) and growth-nucleation rate kinetics in a continuous, gas-phase crystallization system. A specific motivation for such gas-phase studies is the evaluation of the isothermal backmixed reactor as a kinetic tool in the study of other combustion systems which produce particulate products.


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Literature Cited

  1. 1.
    Buckley, H. E., “Crystal Growth,” Chapman and Hall, London (1951).Google Scholar
  2. 2.
    Bunn, Charles, “Crystals: Their Role in Nature and Science,” Academic Press, New York (1964).zbMATHGoogle Scholar
  3. 3.
    Kozlovskii, M. I., Pedagog. Inst. im. T. G. Shevchenko, 4, 109 (1957).Google Scholar
  4. 4.
    Randolph, A. D., and M. A. Larson, AIChE J., 3, No. 5, 639 (1962).CrossRefGoogle Scholar
  5. 5.
    Randolph, A. D., Can. J. Chem. Eng., 42, 280 (1964).CrossRefGoogle Scholar
  6. 6.
    Randolph, A. D., AIChE J., 11, No. 3, 424(1965).CrossRefGoogle Scholar
  7. 7.
    Stone, P. D., M.S. thesis, Univ. Fla., Gainesville (1967).Google Scholar

Copyright information

© Springer Science+Business Media New York 1969

Authors and Affiliations

  • Paul D. Stone
    • 1
  • Alan D. Randolph
    • 1
  1. 1.University of FloridaGainesvilleUSA

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