Skip to main content

Simulation and Experimental Study on the Directional Solidification Process of a Single-Crystal Superalloy Plate Casting

  • Conference paper
  • First Online:
Physics and Engineering of Metallic Materials (CMC 2018)

Part of the book series: Springer Proceedings in Physics ((SPPHY,volume 217))

Included in the following conference series:

  • 1471 Accesses

Abstract

The directional solidification (DS) process and as-cast microstructure of a single-crystal (SX) plate casting were investigated through simulations and experiments. Simulations were conducted to optimize the directional solidification process. The mushy zone showed flat and concave morphology at the withdrawing rate of 3 and 6 mm/min, respectively. Based on the simulation results, the directional solidification experiment was performed at the withdrawing rate of 3 mm/min to achieve a preferable microstructure. On the basis of the start block, many newly formed grains appeared due to the chilling effect of the chilling copper plate. With the increase of location height, these grains continuously coarsened and competed, and the grain density gradually decreased. Only a few grains entered into the spiral selector, and only one grain with the orientation close to [001] preferential orientation could get through it to form the SX structure of the plate casting. From the lower to the upper part of the SX plate casting, the primary dendritic arm spacing first decreased from 467.7 to 435.22 μm, and then increased to 565.81 μm; the secondary dendritic arm spacing increased by 11.4%, from 181.39 to 202.13 μm. The γ′ phases in the dendritic arms showed a cubical morphology, and some micropores appeared near the eutectic particles. The simulated grain structure evolutions conformed well with the experiments.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 189.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Hardcover Book
USD 249.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. J.H. Perepezko, The hotter the engine, the better. Science 326(5956), 1068–1069 (2009)

    Article  CAS  Google Scholar 

  2. R.C. Reed, The superalloys fundamentals and applications (Cambridge University Press, New York, 2006)

    Book  Google Scholar 

  3. M.M. Franke, R.M. Hilbinger, A. Lohmüller, R.F. Singer, The effect of liquid metal cooling on thermal gradients in directional solidification of superalloys: thermal analysis. J. Mater. Process. Technol. 213(12). 2081–2088 (2013)

    Article  CAS  Google Scholar 

  4. J.D. Miller, T.M. Pollock, Stability of dendrite growth during directional solidification in the presence of a non-axial thermal field. Acta Mater. 78, 23–36 (2014)

    Article  CAS  Google Scholar 

  5. J.D. Miller, L. Yuan, P.D. Lee, T.M. Pollock, Simulation of diffusion-limited lateral growth of dendrites during solidification via liquid metal cooling. Acta Mater. 69, 47–59 (2014)

    Article  CAS  Google Scholar 

  6. H. Zhang, Q. Xu, B. Liu, Numerical simulation and optimization of directional solidification process of single crystal superalloy casting. Materials 7(3), 1625–1639 (2014)

    Article  Google Scholar 

  7. D. Ma, P.R. Sahm, Primary spacing in directional solidification. Metall. Mater. Trans. 29A, 1113–1119 (1998)

    Article  CAS  Google Scholar 

  8. F. Wang, D.X. Ma, J. Zhang, S. Bogner, A. Bührig-Polaczek, A high thermal gradient directional solidification method for growing superalloy single crystals. J. Mater. Process. Technol. 214(12), 3112–3121 (2014)

    Article  CAS  Google Scholar 

  9. F. Wang, D. Ma, J. Zhang, S. Bogner, A. Bührig-Polaczek, Solidification behavior of a Ni-based single crystal CMSX-4 superalloy solidified by downward directional solidification process. Mater. Charact. 101, 20–25 (2015)

    Article  CAS  Google Scholar 

  10. F. Wang, D. Ma, J. Zhang, L. Liu, J. Hong, S. Bogner, A. Bührig-Polaczek, Effect of solidification parameters on the microstructures of superalloy CMSX-6 formed during the downward directional solidification process. J. Cryst. Growth 389, 47–54 (2014)

    Article  CAS  Google Scholar 

  11. F. Wang, D. Ma, J. Zhang, A. Bührig-Polaczek, Investigation of segregation and density profiles in the mushy zone of CMSX-4 superalloys solidified during downward and upward directional solidification processes. J. Alloy. Compd. 620, 24–30 (2015)

    Article  CAS  Google Scholar 

  12. F. Wang, D. Ma, J. Zhang, L. Liu, S. Bogner, A. Bührig-Polaczek, Effect of local cooling rates on the microstructures of single crystal CMSX-6 superalloy: a comparative assessment of the bridgman and the downward directional solidification processes. J. Alloy. Compd. 616, 102–109 (2014)

    Article  CAS  Google Scholar 

  13. X. Yang, D. Ness, P.D. Lee, N. D’Souza, Simulation of stray grain formation during single crystal seed melt-back and initial withdrawal in the Ni-base superalloy CMSX-4. Mater. Sci. Eng. A413414, 571–577 (2005)

    Article  Google Scholar 

  14. D. Szeliga, K. Kubiak, J. Sieniawski, Control of liquidus isotherm shape during solidification of Ni-based superalloy of single crystal platforms. J. Mater. Process. Technol. 234, 18–26 (2016)

    Article  CAS  Google Scholar 

  15. X.B. Meng, J.G. Li, Z.Q. Chen, Y.H. Wang, S.Z. Zhu, X.F. Bai, F. Wang, J. Zhang, T. Jin, X.F. Sun, Z.Q. Hu, Effect of platform dimension on the dendrite growth and stray grain formation in a Ni-base single-crystal superalloy. Metall. Mater. Trans. 44A, 1955–1965 (2012)

    Google Scholar 

  16. X.B. Meng, J. Li, S. Zhu, H. Du, Z. Yuan, J. Wang, T. Jin, X. Sun, Z. Hu, Method of stray grain inhibition in the platforms with different dimensions during directional solidification of a Ni-base superalloy. Metall. Mater. Trans. 45A, 1230–1237 (2013)

    Google Scholar 

  17. R. Wang, X. Yan, Z. Li, Q. Xu, B. Liu, Effect of construction manner of mould cluster on stray grain formation in dummy blade of DD6 superalloy. High Temp. Mater. Processes 36(4), 399–409 (2017)

    Article  CAS  Google Scholar 

  18. J. Hong, D. Ma, J. Wang, F. Wang, A. Dong, B. Sun, A. Bührig-Polaczek, Geometrical effect of freckle formation on directionally solidified superalloy CM247 LC components. J. Alloys Compd. 648, 1076–1082 (2015)

    Article  CAS  Google Scholar 

  19. D. Ma, A.B. Polaczed, The influence of surface roughness on freckle formation in directionally solidified superalloy samples. Metall. Mater. Trans. 43B, 671–677 (2012)

    Article  Google Scholar 

  20. D. Ma, Q. Wu, B.P. Andreas, Some new observations on freckle formation in directionally solidified superalloy components. Metall. Mater. Trans. 43B, 344–357 (2012)

    Article  Google Scholar 

  21. J.W. Aveson, P.A. Tennant, B.J. Foss, B.A. Shollock, H.J. Stone, N. D′ Souza, On the origin of sliver defects in single crystal investment castings. Acta Mater. 61(14), 5162–5171 (2013)

    Article  CAS  Google Scholar 

  22. L. Cao, L. Yao, Y. Zhou, T. Jin, X. Sun, Formation of the surface eutectic of a Ni-based single crystal superalloy. J. Mater. Sci. Technol. 33(4), 347–351 (2017)

    Article  Google Scholar 

  23. H.N. Mathur, C. Panwisawas, C.N. Jones, R.C. Reed, C.M.F. Rae, Nucleation of recrystallisation in castings of single crystal Ni-based superalloys. Acta Mater. 129, 112–123 (2017)

    Article  CAS  Google Scholar 

  24. C. Panwisawas, H. Mathur, J. Gebelin, D. Putman, C.M.F. Rae, R.C. Reed, Prediction of recrystallization in investment cast single-crystal superalloys. Acta Mater. 61(1), 51–66 (2013)

    Article  CAS  Google Scholar 

  25. L.H. Rettberg, T.M. Pollock, Localized recrystallization during creep in nickel-based superalloys GTD444 and René N5. Acta Mater. 73, 287–297 (2014)

    Article  CAS  Google Scholar 

Download references

Acknowledgements

This research was funded by the National Science and Technology Major Project (2017ZX04014001) and National Key R&D Program of China (2017YFB0701503).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Qingyan Xu .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2019 Springer Nature Singapore Pte Ltd.

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Wang, R., Xu, Q., Liu, B. (2019). Simulation and Experimental Study on the Directional Solidification Process of a Single-Crystal Superalloy Plate Casting. In: Han, Y. (eds) Physics and Engineering of Metallic Materials. CMC 2018. Springer Proceedings in Physics, vol 217. Springer, Singapore. https://doi.org/10.1007/978-981-13-5944-6_36

Download citation

  • DOI: https://doi.org/10.1007/978-981-13-5944-6_36

  • Published:

  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-13-5943-9

  • Online ISBN: 978-981-13-5944-6

  • eBook Packages: Physics and AstronomyPhysics and Astronomy (R0)

Publish with us

Policies and ethics