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Verbindungen mit Fluor und Sauerstoff

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Niob

Part of the book series: Nb. Niob. Niobium (System-Nr. 49) ((2021,volume N-b / B / 4))

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Zusammenfassung

Die Verbindung wird dargestellt durch 50stündiges Erhitzen von NbO2 mit überschüssigem LiF (Molverhältnis 1:5) auf 800°C in H2-Atmosphäre oder Vakuum und Auswaschen mit H2O; die Verbindung enthält dann noch etwa 5% NbO2. LiNbO2F ist nach Pulveraufnahmen rhomboedrisch mit a = 5.485 Å und α = 55.92°C, bei hexagonaler Indizierung a = 5.144, c =13.835 Å. Paramagnetisch; für diamagnetische Anteile korrigierte Suszeptibilität des Nb4+-Ions χ = 40 × 106. Spezifische elektrische Leitfähigkeit x = 2 × 10−7Ω−1 · cm−1 nach Messungen unter 800 kg · cm−2 Druck, W. Rüdorff, D. Krug (Z. Anorg. Allgem. Chem. 329 [1964] 211/7).

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  1. Herbert Lehl
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Herbert Lehl

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© 1972 Springer-Verlag Berlin Heidelberg

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Lehl, H. (1972). Verbindungen mit Fluor und Sauerstoff. In: Lehl, H. (eds) Niob. Nb. Niob. Niobium (System-Nr. 49), vol N-b / B / 4. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-11109-3_10

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  • DOI: https://doi.org/10.1007/978-3-662-11109-3_10

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-662-11110-9

  • Online ISBN: 978-3-662-11109-3

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