Abstract
The 2D exchange MAS NMR experiment for detecting ultraslow molecular dynamics and the rotor-synchronized 2D experiment for studying the degree of molecular orientation in partially ordered solids are combined into a rotor-synchronized 3D experiment, which correlates molecular order and dynamics. The experiment is outlined and demonstrated experimentally on highly oriented poly (oxymethylene), POM.
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Y. Yang, A. Hagemeyer, H.W. Spiess, Macromolecules 22, 1004 (1989).
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© 1990 Springer-Verlag Berlin Heidelberg
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Yang, Y., Hagemeyer, A., Zemke, K., Spiess, H.W. (1990). 3D 13C MAS NMR Experiment Correlating Order and Dynamics. In: Mehring, M., von Schütz, J.U., Wolf, H.C. (eds) 25th Congress Ampere on Magnetic Resonance and Related Phenomena. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-76072-3_169
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DOI: https://doi.org/10.1007/978-3-642-76072-3_169
Publisher Name: Springer, Berlin, Heidelberg
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