Skip to main content

Sub-rapid Solidification Study of Silicon Steel by Using Dip Test Technique

  • Conference paper
  • First Online:
TMS 2020 149th Annual Meeting & Exhibition Supplemental Proceedings

Part of the book series: The Minerals, Metals & Materials Series ((MMMS))

Abstract

Dip test technique has been used for the study of sub-rapid solidification (cooling rate ranges from 100 ℃/s up to 1000 ℃/s) of molten steel to effectively simulate the thermophysical phenomena during strip casting process due to its convenient and online observation advantages. In this study, a 6.5 wt% Si electric steel strip was produced by an improved dip test apparatus, which has been developed for the research of interfacial heat transfer and microstructure of strip casting steels. The heat transfer rates were calculated by the inverse heat conduction program (IHCP). The analysis of solidification microstructure and second phase precipitation was also carried out by scanning electron microscope (SEM ) and transmission electron microscope (TEM ). The results showed that the maximum heat flux could be up to 8.2 MW/m2, and only a very small amount of MnS (0.5 μm) and AlN (2 μm) precipitates were found in the as-cast strip while nano -size MnS (~50 nm) and TiN (50–200 nm) precipitates were observed with subsequent heat treatment , after which the magnetic properties were also significantly improved.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 169.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 219.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 219.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Takashima M, Komatsubara M, Morito N (1997) {001} <210> texture development by two-stage cold rolling method in non-oriented electrical steel. ISIJ Int 37:1263–1268

    Article  CAS  Google Scholar 

  2. Xia ZS, Kang YL, Wang QL (2008) Developments in the production of grain-oriented electrical steel. J Magn Magn Mater 320:3229–3233

    Article  CAS  Google Scholar 

  3. Takahashi N, Suga Y, Kobayashi H (1996) Recent developments in grain-oriented silicon-steel. J Magn Magn Mater 160:98–101

    Article  CAS  Google Scholar 

  4. Netto PGQ, Tavares RP, Isac M, Guthrie RIL (2001) A technique for the evaluation of instantaneous heat fluxes for the horizontal strip casting of aluminum alloys. ISIJ Int 41(11):1340–1349

    Article  CAS  Google Scholar 

  5. Luiten EEM, Blok K (2003) Stimulating R&D of industrial energy-efficient technology; the effect of government intervention on the development of strip casting technology. Energy Policy 31(13):1339–1356

    Article  Google Scholar 

  6. Park JY, Oh KH, Ra HY (2001) The effects of superheating on texture and microstructure of Fe-4.5 wt% Si steel strip by twin-roll strip casting. ISIJ Int 41:70–75

    Article  CAS  Google Scholar 

  7. Park JY, Oh KH, Ra HY (1999) Microstructure and crystallographic texture of strip-cast 4.3 wt% Si steel sheet. Scr Mater 40:881–885

    Article  CAS  Google Scholar 

  8. Honma H, Ushigami Y, Suga Y (1991) Magnetic properties of (110)[001] grain oriented 6.5% silicon steel. J Appl Phys 70:6259–6261

    Article  CAS  Google Scholar 

  9. Loulou T, Artyukhin EA, Bardon JP (1999) Estimation of thermal contact resistance during the first stages of metal solidification process: I—experiment principle and modelisation. Int J Heat Mass Tran 42(12):2129–2142

    Article  CAS  Google Scholar 

  10. Nolli P, Cramb AW (2008) Naturally deposited oxide films in near-net-shape casting: importance, mechanisms of formation, and prediction. Metall Mater Trans, B 39(B):56–65

    Google Scholar 

  11. Nolli P, Cramb AW (2007) Interaction between iron droplets and H2S during solidification. ISIJ Int 47:1284–1293

    Article  CAS  Google Scholar 

  12. Yu Y, Cramb AW, Heard R, Fang Y, Cui J (2006) The effect of oxygen partial pressure on heat transfer and solidification. ISIJ Int 46(10):1427–1431

    Article  CAS  Google Scholar 

  13. Zhu CY, Wang WL, Lu C (2019) Characterization of cermet coatings and its effect on the responding heat transfer performance in strip casting process. J Alloy Compd 770:631–639

    Article  CAS  Google Scholar 

  14. Wang WL, Zhu CY, Lu C, Yu J, Zhou LJ (2018) Study of the heat transfer behavior and naturally deposited films in strip casting by using droplet solidification technique. Metall Mater Trans, A

    Google Scholar 

  15. Strezov L, Herbertson J (1998) Experimental studies of interfacial heat transfer and initial solidification pertinent to strip casting. ISIJ Int 38:959–966

    Article  CAS  Google Scholar 

  16. Strezov L, Herbertson J, Belton GR (2000) Mechanisms of initial melt/substrate heat transfer pertinent to strip casting. Metall Mater Trans, B 31(B):1023–1030

    Google Scholar 

  17. Jenkins K, Lindenmo M (2008) Precipitates in electrical steels. J Magn Magn Mater 320:2423–2429

    Article  CAS  Google Scholar 

  18. Iwayama K, Haratani T (1980) The dissolution and precipitation behavior of ain and MnS in grain-oriented 3% silicon-steel with high permeability. J Magn Magn Mater 19:15–17

    Article  CAS  Google Scholar 

  19. Fabrício Luiz de ALCÂNTARA (2013) Aluminium nitride precipitation in Fe-3% Si Steel. ISIJ Int 53:1211–1214

    Article  Google Scholar 

  20. Wriedt HA, Hsun HU (1976) The solubility product of manganese sulfide in 3 pct silicon-iron at 1270 to 1670 K. Metall Mater Transactions. A, 7(4):711–718

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Wanlin Wang .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2020 The Minerals, Metals & Materials Society

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Qian, H., Wang, W. (2020). Sub-rapid Solidification Study of Silicon Steel by Using Dip Test Technique. In: TMS 2020 149th Annual Meeting & Exhibition Supplemental Proceedings. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-36296-6_4

Download citation

Publish with us

Policies and ethics