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Optimization of Extraction of Kusum Seed Oil Through Soxhlet Extraction Process Using N-Hexane Solvent

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Techno-Societal 2018

Abstract

As fossil fuels are depleting fast, there is an urgent need to search for alternative fuels. Several experimental studies were conducted on the extraction of oil, trans-esterification and Engine testing on biodiesels by several researchers since the past few years. The Kusum seed oil is one such promising source of oil, and it is a non-edible vegetable oil. However, it was found that very few studies have been conducted so far on this oil. The present work is on the extraction of oil from Kusum seeds by using n-hexane as a solvent in Soxhlet extractor through the chemical extraction process. The major influencing input parameters that affect the yield of KSO are particle size, reaction time, reaction temperature, the volume of extractant and number of cycles. An experimental array L9 was selected for the design of experiments (DOE) with four parameters and three levels and it analyzes using analysis of variance (ANOVA). The oil yield was in between 34% and 39% with the optimal yield of 38.85% for the 6th experimental set.

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Notes

  1. 1.

    All graphs are drawn in Minitab software by considering mean values

References

  1. Silitonga AS, Masjuki HH, Mahlia TMI, Ong HC, Kusumo F, Aditiya HB, Ghazali NNN (2015) Schleichera oleosa L oil as feedstock for biodiesel production. Fuel 156:63–70

    Article  Google Scholar 

  2. Bankovili IB, Stamenkovi OS, Veljkovi VB (2012) Biodiesel production from non-edible plant oils. Renew Sust Energ Rev 16:3621–3647

    Article  Google Scholar 

  3. Janaun J, Ellis N (2010) Perspectives on biodiesel as a sustainable fuel. Renew Sust Energ Rev 14(4):1312–1320

    Article  Google Scholar 

  4. Soo-Young No (2011) Inedible vegetable oils and their derivatives for alternative diesel fuels in CI engines: a review. Renew Sust Energ Rev 15:131–149

    Article  Google Scholar 

  5. Nayaka SK, Pattanaika BP (2013) Experimental investigation on performance and emission characteristics of a diesel engine fuelled with mahua biodiesel using additive. 4th international conference on advances in energy research (ICAER 2013)

    Google Scholar 

  6. Rathod NP, Lawankar SM (2013) Experimental investigation on use of methyl ester Kusum oil and its blends in direct injection CI engine. IOSR J Mech Civil Eng 10(3):36–43

    Article  Google Scholar 

  7. Premananadas, Mohanty RC, Swain D. Non-edible Kusum oil: potential foliage of biodiesel production and its productive use in marine engines. Int J Res Eng Technol 4(9): 25–36

    Google Scholar 

  8. Bhargavi N, Krishna Reddy AV (2014) Performance and emissions analysis of Kusum oil methyl esters with air pre heating on C.I engine. Int J Sci Eng Res 3(9):27

    Google Scholar 

  9. Kumar S, Bhattacharyya B, Gupta VK. Present and future energy scenario in India

    Google Scholar 

  10. Crude Oil Scenario. http://www.mcxcalls.in/crude-oil-scenario/7/7/2018

  11. https://www.scribd.com/document/44645024/Chapter-2-Oil-Extraction. Oil extraction by Timothy G. Kemper

  12. www.yearbook.enerdata.net/ Global Energy Statistical Yearbook 2018

  13. www.mospi.gov.in/ Energy Statistics-2015/National Statistical Organization Ministry of Statistics and Programme Implementation Government of India

  14. www.eia.gov/ U.S. Energy Information Administration/International Energy Statistics, 2014

  15. Bagby M, Freedman B (1987) Preparation and properties from vegetable oils. Fuel 66:1372–1378

    Article  Google Scholar 

  16. BP Statistical Review of World Energy June 2012, 2013, 2014. 68th edn

    Google Scholar 

  17. Government of India Planning Commission (2012) Faster, sustainable and more inclusive growth an approach to the twelfth five-year plan 2012–17

    Google Scholar 

  18. Planning Commission, Government of India (2003) Report of the committee on development of biofuel, 16 April 2003

    Google Scholar 

  19. India Biofuels Annual 2017, approved by: Scott Sindelar, prepared by Amit Aradhey

    Google Scholar 

  20. Pali HS, Kumar N (2012) Kusum oil as a potential fuel for CI Engines. Conference: international conference on alternative fuels for I.C. engines. https://doi.org/10.13140/2.1.3313.6966

  21. Luque de Castro MD, Priego-Capote F Soxhlet extraction: past and present panacea. J Chromatogr 1217(16):2383–2389. https://doi.org/10.1016/j.chroma.2009.11.027

    Article  Google Scholar 

  22. Murmu R, Sutar H, Patra S (2017) Experimental investigation and process optimization of biodiesel production from Kusum oil using Taguchi method. Adv Chem Eng Sci 7:464–476. https://doi.org/10.4236/aces.2017.74033

    Article  Google Scholar 

  23. India Biofuels Annual 2017, approved by: Scott Sindelar, prepared by Amit Aradhey 06/27/2017

    Google Scholar 

  24. Timoty G. Kemper oil extraction. http://www.readbag.com/uqu-sa-files2-tiny-mce-plugins-filemanager-files-4281709-84607-61

  25. Luque de Castro MD, Priego-Capote F (2010) Review on Soxhlet extraction: past and present panacea. J Chromatogr A 1217(16):2383–2389. https://doi.org/10.1016/j.chroma.2009.11.027

    Article  Google Scholar 

  26. Poshetti AG. Biodiesel production process optimization and CI engine performance analysis using Kusum biodiesel. MTech report, DBATU, 2016–17

    Google Scholar 

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Sonage, S., Warake, S., Barde, D., Chaudhari, K., Jawale, U., Tandale, M. (2020). Optimization of Extraction of Kusum Seed Oil Through Soxhlet Extraction Process Using N-Hexane Solvent. In: Pawar, P., Ronge, B., Balasubramaniam, R., Vibhute, A., Apte, S. (eds) Techno-Societal 2018 . Springer, Cham. https://doi.org/10.1007/978-3-030-16848-3_29

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