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An Investigation of Detwinning Behavior of In-plane Compressed E-form Mg Alloy During the In Situ Tensile Test

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Magnesium Technology 2019

Part of the book series: The Minerals, Metals & Materials Series ((MMMS))

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Abstract

In this study, we investigated the detwinning phenomenon of in-plane compressed E-form magnesium (Mg) alloy sheet systematically using in situ tensile test combined with electron backscattered diffraction (EBSD ) technique. Microstructure and microtexture evolutions were analyzed at different tensile strains during the in situ tensile test . The detwinning phenomenon in E-form Mg alloy was found to be linked to both twin boundary mobility and the interaction of their boundaries with dislocations. The pre-compressed sheet of E-form Mg alloy effectively accommodated the thickness direction strains generated during the in situ tensile test . The effect of detwinning on formability and mechanical behavior of the E-form Mg alloy was also examined. EBSD results indicate that most of the deformation twins formed during in-plane compression were removed when the load is reversed during the in situ tensile test .

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References

  1. Polmear IJ (1994) Magnesium alloys and applications. Mater. Sci. Technol. 10: 1–16. https://doi.org/10.1179/026708394790163401

    Article  CAS  Google Scholar 

  2. Aslam I, Li B, McClelland Z, Horstemeyer SJ, Ma Q, Wang PT, Horstemeyer MF (2014) Three-point bending behavior of a ZEK100 Mg alloy at room temperature. Mater. Sci. Eng. A 590: 168–173. https://doi.org/10.1016/j.msea.2013.10.030

    Article  CAS  Google Scholar 

  3. Huang X, Suzuki K, Saito N (2009) Textures and stretch formability of Mg-6Al-1Zn magnesium alloy sheets rolled at high temperatures up to 793 K. Scr. Mater. 60: 651–654. https://doi.org/10.1016/j.scriptamat.2008.12.035

    Article  CAS  Google Scholar 

  4. Wenwen D, Yangshan S, Xuegang M, Feng X, Min Z, Dengyun W (2003) Microstructure and mechanical properties of Mg-Al based alloy with calcium and rare earth additions. Mater. Sci. Eng. A 356: 1–7. https://doi.org/10.1016/s0921-5093(02)00551-8

    Article  Google Scholar 

  5. Wang L, Huang G, Han T, Mostaed E, Pan F, Vedani M (2015) Effect of twinning and detwinning on the spring-back and shift of neutral layer in AZ31 magnesium alloy sheets during V-bend. Mater. Des. 68: 80–87. https://doi.org/10.1016/j.matdes.2014.12.017

    Article  CAS  Google Scholar 

  6. Park SH, Hong SG, Lee CS (2013) Enhanced stretch formability of rolled Mg-3Al-1Zn alloy at room temperature by initial {10–12} twins. Mater. Sci. Eng. A 578: 271–276. https://doi.org/10.1016/j.msea.2013.04.084

    Article  CAS  Google Scholar 

  7. He W, Zeng Q, Yu H, Xin Y, Luan B, Liu Q (2016) Improving the room temperature stretch formability of a Mg alloy thin sheet by pre-twinning. Mater. Sci. Eng. A 655: 1–8. https://doi.org/10.1016/j.msea.2015.12.070

    Article  CAS  Google Scholar 

  8. Jiang L, Jonas JJ, Luo AA, Sachdev AK, Godet S (2007) Influence of {10-12} extension twinning on the flow behavior of AZ31 Mg alloy. Mater. Sci. Eng. A 445–446: 302–309. https://doi.org/10.1016/j.msea.2006.09.069

    Article  Google Scholar 

  9. Xin Y, Wang M, Zeng Z, Nie M, Liu Q (2012) Strengthening and toughening of magnesium alloy by {10-12} extension twins. Scr. Mater. 66: 25–28. https://doi.org/10.1016/j.scriptamat.2011.09.033

    Article  CAS  Google Scholar 

  10. Knezevic M, Levinson A, Harris R, Mishra RK, Doherty RD, Kalidindi SR (2010) Deformation twinning in AZ31: Influence on strain hardening and texture evolution. Acta Mater. 58: 6230–6242. https://doi.org/10.1016/j.actamat.2010.07.041

    Article  CAS  Google Scholar 

  11. Wu W, Gao Y, Li N, Parish CM, Liu W, Liaw PK, An K (2016) Intragranular twinning, detwinning, and twinning-like lattice reorientation in magnesium alloys. Acta Mater. 121: 15–23. https://doi.org/10.1016/j.actamat.2016.08.058

    Article  CAS  Google Scholar 

  12. Li Y, Cui Y, Bian H, Sun S, Tang N, Chen Y, Liu B, Koizumi Y, Chiba A (2014) Detwining in Mg alloy with a high density of twin boundaries. Sci. Technol. Adv. Mater. 15: 035003. https://doi.org/10.1088/1468-6996/15/3/035003

    Article  Google Scholar 

  13. Hama T, Kitamura N, Takuda H (2013) Effect of twinning and detwinning on inelastic behavior during unloading in a magnesium alloy sheet. Mater. Sci. Eng. A 583: 232–241. https://doi.org/10.1016/j.msea.2013.06.070

    Article  CAS  Google Scholar 

  14. Yin SM, Yang F, Yang XM, Wu SD, Li SX, Li GY (2008) The role of twinning-detwinning on fatigue fracture morphology of Mg-3%Al-1%Zn alloy. Mater. Sci. Eng. A 494: 397–400. https://doi.org/10.1016/j.msea.2008.04.056

    Article  Google Scholar 

  15. Dong S, Yu Q, Jiang Y, Dong J, Wang F, Ding W (2015) Electron backscatter diffraction observations of twinning-detwinning evolution in a magnesium alloy subjected to large strain amplitude cyclic loading. Mater. Des. 65: 762–765. https://doi.org/10.1016/j.matdes.2014.09.079

    Article  CAS  Google Scholar 

  16. Hama T, Tanaka Y, Uratani M, Takuda H (2016) Deformation behavior upon two-step loading in a magnesium alloy sheet. Int. J. Plast. 82: 283–304. https://doi.org/10.1016/j.ijplas.2016.03.009

    Article  CAS  Google Scholar 

  17. Culbertson D, Yu Q, Wang J, Jiang Y (2017) Pre-compression effect on microstructure evolution of extruded pure polycrystalline magnesium during reversed tension load. Mater. Charact. 134: 41–48. https://doi.org/10.1016/j.matchar.2017.10.003

    Article  CAS  Google Scholar 

  18. Song B, Guo N, Liu T, Yang Q (2014) Improvement of formability and mechanical properties of magnesium alloys via pre-twinning: A review. Mater. Des. 62: 352–360. https://doi.org/10.1016/j.matdes.2014.05.034

    Article  CAS  Google Scholar 

  19. Singh J, Kim M-S, Choi S-H (2017) The effect of strain heterogeneity on the deformation and failure behaviors of E-form Mg alloy sheets during a mini-V-bending test. J. Alloys Compd. 708: 694–705. https://doi.org/10.1016/j.jallcom.2017.02.176

    Article  CAS  Google Scholar 

  20. Singh J, Kim M-S, Choi S-H (2018) The effect of initial texture on micromechanical deformation behaviors in Mg alloys under a mini-V-bending test. Int. J. Plast. https://doi.org/10.1016/j.ijplas.2018.01.008

  21. Singh J, Kim M-S, Lee S-E, Kim E-Y, Kang J-H, Park J-H, Kim J-J, Choi S-H (2018) Heterogeneity in deformation and twinning behaviors through the thickness direction in E-form Mg alloy sheets during an Erichsen test. Mater. Sci. Eng. A 729: 370–384. https://doi.org/10.1016/j.msea.2018.05.072

    Article  CAS  Google Scholar 

  22. Lee MG, Kim JH, Kim D, Seo OS, Nguyen NT, Kim HY (2013) Anisotropic Hardening of Sheet Metals at Elevated Temperature: Tension-Compressions Test Development and Validation. Exp. Mech. 53: 1039–1055. https://doi.org/10.1007/s11340-012-9694-1

    Article  Google Scholar 

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Acknowledgements

This research was supported by the National Research Foundation of Korea (NRF) funded by the Ministry of Science and ICT, Government of Korea (NRF-2016M3C1B5906955), and the Basic Science Research Program through the NRF funded by the Ministry of Education, Government of Korea (NRF-2014R1A6A1030419).

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Correspondence to Shi-Hoon Choi .

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Singh, J., Kim, MS., Lee, SE., Kang, JH., Choi, SH. (2019). An Investigation of Detwinning Behavior of In-plane Compressed E-form Mg Alloy During the In Situ Tensile Test. In: Joshi, V., Jordon, J., Orlov, D., Neelameggham, N. (eds) Magnesium Technology 2019. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-05789-3_30

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