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Characterization of Minerals, Metals, and Materials 2019 pp 225–235Cite as

Microwave-Assisted Solid-State Synthesis of Fluorinated Hydroxyapatite

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Part of the book series: The Minerals, Metals & Materials Series ((MMMS))

Abstract

As an important inorganic component of vertebrate bones and teeth, hydroxyapatite (HA) has excellent biocompatibility, bioactivity, osteoconductivity and chemical stability, and can be used as a drug-release carrier and bone tissue engineering repair material. However, when it is used alone, it often presents a few disadvantages such as large brittleness, low fatigue resistance, and easy agglomeration. In this study, to improve its mechanical properties fluorinated hydroxyapatite (FHA) was synthesized by doping fluorine ion in nanocrystalline HA in solid state through microwave sintering of the mixture of HA and MgF2 in the presence of water as an adhesive agent. The X-ray diffraction (XRD ), scanning electron microscopy (SEM ), and Fourier-transform infrared spectroscopy (FTIR) analyses were performed to explore the formation mechanism of FHA from HA under microwave irradiation.

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Acknowledgements

This work was partially supported by the Fundamental Research Funds for the Central Universities of Central South University under Grant 2018zzts040, the Co-Innovation Center for Clean and Efficient Utilization of Strategic Metal Mineral Resources under Grant 2014-405, the Innovation-Driven Program of Central South University under Grant 2016CXS021, and the Shenghua Lieying Program of Central South University under Grant 502035001.

Author information

Authors and Affiliations

  1. Xiangya Stomatological Hospital, Central South University, Changsha, 410008, Hunan, China

    Qian Peng & Zhangui Tang

  2. School of Xiangya Stomatology, Central South University, Changsha, 410008, Hunan, China

    Qian Peng & Zhangui Tang

  3. School of Minerals Processing and Bioengineering, Central South University, Changsha, 410083, Hunan, China

    Huimin Tang & Zhiwei Peng

Authors
  1. Qian Peng
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  2. Huimin Tang
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  3. Zhangui Tang
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  4. Zhiwei Peng
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Corresponding authors

Correspondence to Zhangui Tang or Zhiwei Peng .

Editor information

Editors and Affiliations

  1. Michigan Technological University, Houghton, MI, USA

    Bowen Li

  2. CanmetMATERIALS, Hamilton, ON, Canada

    Jian Li

  3. Al-Isra University, Amman, Jordan

    Shadia Ikhmayies

  4. ArcelorMittal Global R&D, East Chicago, IN, USA

    Mingming Zhang

  5. Middle East Technical University, Ankara, Turkey

    Yunus Eren Kalay

  6. Los Alamos National Laboratory, Los Alamos, NM, USA

    John S. Carpenter

  7. Michigan Technological University, Houghton, MI, USA

    Jiann-Yang Hwang

  8. Military Institute of Engineering, Rio de Janeiro, Brazil

    Sergio Neves Monteiro

  9. Chongqing University, Chongqing, China

    Chenguang Bai

  10. UNSW Canberra, Campbell, ACT, Australia

    Juan P. Escobedo-Diaz

  11. Free University of Bozen-Bolzano, Bolzano, Italy

    Pasquale Russo Spena

  12. Naval Research Laboratory, Washington, DC, USA

    Ramasis Goswami

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© 2019 The Minerals, Metals & Materials Society

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Peng, Q., Tang, H., Tang, Z., Peng, Z. (2019). Microwave-Assisted Solid-State Synthesis of Fluorinated Hydroxyapatite. In: Li, B., et al. Characterization of Minerals, Metals, and Materials 2019. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-05749-7_23

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