Abstract
This chapter discusses some of the most important imaging methods with low-energy electrons, including: low-energy electron microscopy ( ), its extension to spin-polarized low-energy electron microscopy ( ), and its combination with spectroscopic photoemission and low-energy electron microscopy ( ). Other imaging methods mentioned only briefly in the chapter include ultraviolet photoemission electron microscopy ( ), mirror electron microscopy () , low-electron energy loss microscopy ( ), and Auger electron emission microscopy ( ). The instruments used in these imaging methods allow imaging not only in real space but also in reciprocal space, such as low-energy electron diffraction ( ) and angle-resolved photoelectron spectroscopy (ARPES in SPELEEM). The combination of these methods with complementary high-lateral-resolution methods renders imaging with low-energy electrons a comprehensive surface analysis tool.
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R. Zdyb, E. Bauer: Spin-resolved inelastic mean free path of slow electrons in Fe, J. Phys. Condens. Matter 25, 272201 (2013)
Y.Z. Wu, A.K. Schmid, Z.Q. Qiu: Spin-dependent quantum interference from epitaxial MgO thin films on Fe(001), Phys. Rev. Lett. 97, 217205 (2006)
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T. Duden, E. Bauer: Magnetic domain structure and spin reorientation transition in the system Co/Au/W(110), MRS Proceedings 475, 283 (1997)
F. El Gabaly, S. Gallego, C. Muñoz, L. Szunyogh, P. Weinberger, C. Klein, A.K. Schmid, K.F. McCarty, J. de la Figuera: Imaging spin-reorientation transitions in consecutive atomic Co layers on Ru(0001), Phys. Rev. Lett. 96, 147202 (2006)
C. Klein, R. Ramchal, M. Farle, A.K. Schmid: Direct imaging of spin-reorientation transitions in ultrathin Ni films by spin-polarized low-energy electron microscopy, Surf. Interface Anal. 38, 1550–1553 (2006)
C. Klein, R. Ramchal, A.K. Schmid, M. Farle: Controlling the kinetic order of spin-reorientation transitions in Ni/Cu(100) films by tuning the substrate step structure, Phys. Rev. B 75, 193405 (2007)
F. El Gabaly, K.F. McCarty, A.K. Schmid, J. de la Figuera, M.C. Muñoz, L. Szunyogh, P. Weinberger, S. Gallego: Noble metal capping effects on the spin-reorientation transitions of Co/Ru(0001), New J. Phys. 10, 073024 (2008)
B. Santos, S. Galego, A. Mascaraque, K.F. McCarty, A. Quesada, A.T. N'Diaye, A.K. Schmid, J. de la Figuera: Hydrogen-induced reversible spin-reorientation transition and magnetic stripe domain phase in bilayer Co on Ru(0001), Phys. Rev. B 85, 134409 (2012)
Q. Wu, M.S. Altman: Spin polarized low energy electron microscopy of quantum well resonances in Fe films on the Cu-covered W(110) surface, Ultramicroscopy 130, 109–114 (2013)
Q. Wu, M.S. Altman: Probing buried magnetic interface structure with the quantum size effect in spin-dependent electron reflectivity, Ultramicroscopy 159, 530–535 (2015)
K.L. Man, M.S. Altman, H. Poppa: Spin polarized low energy electron microscopy investigations of magnetic transitions in Fe/Cu(100), Surf. Sci. 480, 163–172 (2001)
K.L. Man, W.L. Ling, S.Y. Paik, H. Poppa, M.S. Altman, Z.Q. Qiu: Modification of initial growth and magnetism in Fe/Cu(100), Phys. Rev. B 65, 024409 (2001)
H. Poppa, E.D. Tober, A.K. Schmid: In situ observation of magnetic domain pattern evolution in applied fields by spin-polarized low energy electron microscopy, J. Appl. Phys. 91, 6932–6934 (2002)
R. Zdyb, E. Bauer: Magnetic domain structure and spin reorientation transition in ultrathin Fe-Co alloy films, Phys. Rev. B 67, 134420 (2003)
R. Zdyb, A. Locatelli, S. Heun, S. Cherifi, R. Belkhou, E. Bauer: Nanomagnetism studies with spin-polarized low energy electron microscopy and x-ray magnetic circular dichroism photo emission electron microscopy, Surf. Interface Anal. 27, 239–243 (2005)
C. Ji, Z. Wang, Q. Wu, L. Huang, M.S. Altman: Controlling magnetic interfaces using ordered surface alloys, Phys. Rev. B 94, 134425 (2016)
T. Duden, R. Zdyb, M. Altman, E. Bauer: Micromagnetic and microcrystalline structure of ultrathin co layers on W single crystal surfaces, Surf. Sci. 480, 145–152 (2001)
K.L. Man, R. Zdyb, Y.I. Feng, T. Chan, M.S. Altman, E. Bauer: Growth morphology, structure and magnetism of ultrathin co films on W(111), Phys. Rev. B 67, 184402 (2003)
Q. Wu, R. Zdyb, E. Bauer, M.S. Altman: Growth, magnetism and ferromagnetic thickness gap in Fe films on the W(111) surface, Phys. Rev. B 87, 104410 (2013)
Y.R. Niu, K.L. Man, A. Pavlovska, E. Bauer, M.S. Altman: Fe on W(001): From continuous films to nanoparticles: Growth and magnetic domain structure, Phys. Rev. B 95, 064404 (2017)
T. Duden, E. Bauer: Biquadratic exchange in ferromagnetic/nonferromagnetic sandwiches: A spin-polarized low energy electron study, Phys. Rev. B 59, 474–479 (1999)
T. Duden, E. Bauer: Exchange coupling in Co/Cu/Co sandwiches studied by spin-polarized low energy electron microscopy, J. Magn. Magn. Mater. 191, 301–312 (1999)
N. Rougemaille, M. Portalupi, A. Brambilla, P. Biagioni, A. Lanzara, M. Finazzi, A.K. Schmid, L. Duò: Exchange-induced frustration in Fe/NiO multilayers, Phys. Rev. B 76(6), 214425–214421 (2007)
M. Suzuki, T. Yasue, T. Koshikawa, E. Bauer: Magnetic structure of Co/Ni thin film magnetic structure of Co/Ni thin films on W(110) studied by high brightness and highly spin-polarized LEEM. In: Proc. 8th Int. Symp. At. Level Charact. New Mater. Devices ALC'11, Seoul (2011) pp. 437–440
M. Suzuki, K. Kudo, K. Kojima, T. Yasue, N. Akutsu, W.A. Diño, H. Kasai, E. Bauer, T. Koshikawa: Magnetic domain patterns on strong perpendicular magnetization of Co/Ni multilayers as spintronics materials: I. Dynamic observations, J. Phys. Condens. Matter 25, 406001 (2013)
K. Kudo, M. Suzuki, K. Kojima, T. Yasue, N. Akutsu, W.A. Diño, H. Kasai, E. Bauer, T. Koshikawa: Magnetic domain patterns on strong perpendicular magnetization of Co/Ni multilayers as spintronics materials: II. Numerical simulations, J. Phys. Condens. Matter 25, 395005 (2013)
N. Rougemaille, A.T. N'Diaye, J. Coraux, C. Vo-Van, O. Fruchart, A.K. Schmid: Perpendicular magnetic anisotropy of cobalt films intercalated under graphene, Appl. Phys. Lett. 101, 142403 (2012)
H. Yang, A.D. Vu, A. Hallal, N. Rougemaille, J. Coraux, G. Chen, A.K. Schmid, M. Chshiev: Anatomy and giant enhancement of the perpendicular magnetic anisotropy of cobalt-graphene heterostructures, Nano Lett. 16, 145–151 (2016)
A.D. Vu, J. Coraux, G. Chen, A.T. N'Diaye, A.K. Schmid, N. Rougemaille: Unconventional magnetisation texture in graphene/cobalt hybrids, Sci. Rep. 6, 24783 (2016)
R. Ramchal, A.K. Schmid, M. Farle, H. Poppa: Magnetic domains and domain-wall structure in Ni/Cu(001) films imaged by spin-polarized low-energy electron microscopy, Phys. Rev. B 68, 054418 (2003)
G. Chen, J. Zhu, A. Quesada, J. Li, A.T. N'Diaye, Y. Huo, T.P. Ma, Y. Chen, H.Y. Kwon, C. Won, Z.Q. Qiu, A.K. Schmid, Y.Z. Wu: Novel chiral magnetic domain wall structure in Feo/Ni/Cu(001) films, Phys. Rev. Lett. 110, 177204 (2013)
G. Chen, T. Ma, A.T. N'Diaye, H. Kwon, C. Won, Y. Wu, A.K. Schmid: Tailoring the chirality of magnetic domain walls by interface engineering, Nat. Commun. 4, 2671 (2013)
G. Chen, A.T. N'Diaye, Y. Wu, A.K. Schmid: Ternary superlattice boosting interface-stabilized magnetic chirality, Appl. Phys. Lett. 106, 062402 (2015)
G. Chen, A.T. N'Diaye, S.P. Kang, H.Y. Kwon, C. Won, Y. Wu, Z.Q. Qiu, A.K. Schmid: Unlocking Bloch-type chirality in ultrathin magnets through uniaxial strain, Nat. Commun. 6, 6598 (2015)
G. Chen, A. Mascaraque, A.T. N'Diaye, A.K. Schmid: Room temperature skyrmion ground state stabilized through interlayer exchange coupling, Appl. Phys. Lett. 106, 242404 (2015)
G. Chen, A.K. Schmid: Imaging and tailoring the chirality of domain walls in magnetic films, Adv. Mater. 27, 5738–5743 (2015)
E. Bauer, R. Belkhou, S. Cherifi, R. Hertel, S. Heun, A. Locatelli, A. Pavlovska, R. Zdyb, N. Agarwal, H. Wang: Microscopy of mesoscopic ferromagnetic systems with slow electrons, Surf. Interface Anal. 38, 1622–1627 (2006)
R. Zdyb, A. Pavlovska, M. Jałochowski, E. Bauer: Self-organized Fe nanostructures on W(110), Surf. Sci. 600, 1586–1591 (2006)
N. Rougemaille, A.K. Schmid: Self-organization and magnetic domain microstructure of Fe nanowire arrays, J. Appl. Phys. 99, 08S502 (2006)
H.F. Ding, A.K. Schmid, D. Li, K.Y. Guslienko, S.D. Bader: Magnetic bistability of Co nanodots, Phys. Rev. Lett. 94, 157202 (2005)
R. Zdyb, E. Bauer: Coexistence of ferromagnetism and paramagnetism in a ferromagnetic monolayer, Phys. Rev. Lett. 100, 155704 (2008)
J. de la Figuera, Z. Novotny, M. Setvin, T. Liu, Z. Mao, G. Chen, A.T. N'Diaye, M. Schmid, U. Diebold, A.K. Schmid, G.S. Parkinson: Real-space imaging of the Verwey transition at the (100) surface of magnetite, Phys. Rev. B 88, 161410(R) (2013)
J. de la Figuera, L. Vergara, A.T. N'Diaye, A. Quesada, A.K. Schmid: Micromagnetism in (001) magnetite by spin-polarized low-energy electron microscopy, Ultramicroscopy 130, 77–81 (2013)
T.O. Menteş, A. Locatelli: Angle-resolved x-ray photoemission electron microscopy, J. Electron Spectrosc. Relat. Phenom. 185, 323–329 (2012)
A. Locatelli, L. Aballe, T.O. Menteş, M. Kiskinova, E. Bauer: Photoemission electron microscopy with chemical sensitivity: SPELEEM methods and applications, Surf. Interface Anal. 38, 1554–1557 (2006)
T.O. Menteş, M.A. Niño, A. Locatelli: Spectromicroscopy with low-energy electrons: LEEM and XPEEM studies at the nanoscale, e-J. Surf. Sci. Nanotechnol. 9, 72–79 (2011)
E. Bauer, S. Cherifi, L. Daeweritz, M. Kaestner, S. Heun, A. Locatelli: Low-energy electron microscopy/x-ray magnetic circular dichroism photoemission electron microscopy study of epitaxial MnAs on GaAs, J. Vac. Sci. Technol. B 20, 2539–2542 (2002)
E. Bauer, R. Belkhou, S. Cherifi, A. Locatelli, A. Pavlovska, N. Rougemaille: Magnetostructure of MnAs on GaAs revisited, J. Vac. Sci. Technol. B 25, 1470–1475 (2007)
A.B. Pang, A. Pavlovska, L. Däweritz, A. Locatelli, E. Bauer, M.S. Altman: LEEM image phase contrast of MnAs stripes, Ultramicroscopy 130, 7–12 (2013)
R. Engel-Herbert, D.M. Schaadt, S. Cherifi, E. Bauer, R. Belkhou, A. Locatelli, S. Heun, A. Pavlovska, J. Mohanty, K.H. Ploog, T. Hesjedal: The nature of charged zig-zag domains in MnAs thin films, J. Magn. Magn. Mater. 305, 457–463 (2006)
R. Engel-Herbert, T. Hesjedal: Micromagnetic analysis of unusual, V-shaped domain transitions in MnAs nanowires, J. Magn. Magn. Mater. 323, 1840–1845 (2011)
K.S.R. Menon, S. Mandal, J. Das, T.O. Menteş, M.A. Niño, A. Locatelli, R. Belkhou: Surface antiferromagnetic domain imaging using low-energy unpolarized electrons, Phys. Rev. B 84, 132402 (2011)
R. Hertel, O. Fruchart, S. Cherifi, P.-O. Jubert, S. Heun, A. Locatelli, J. Kirschner: Three-dimensional magnetic-flux-closure patterns in mesoscopic Fe islands, Phys. Rev. B 72(11), 214409–214401 (2005)
A. Mascaraque, L. Aballe, J.F. Marco, T.O. Menteş, F. El Gabaly, C. Klein, A.K. Schmid, K.F. McCarty, A. Locatelli, J. de la Figuera: Measuring the magnetization of three monolayer thick Co islands and films by x-ray dichroism, Phys. Rev. B 80, 172401 (2009)
M. Monti, B. Santos, A. Mascaraque, O.R. de la Fuente, M.A. Niño, T.O. Menteş, A. Locatelli, K.F. McCarty, J.F. Marco, J. de la Figuera: Magnetism in nanometer-thick magnetite, Phys. Rev. B 85, 020404 (2012)
T.O. Menteş, A. Locatelli, L. Aballe, A. Pavlovska, E. Bauer, T. Pabisiak, A. Kiejna: Surface modification of oxides by electron-stimulated desorption for growth-mode control of metal films: Experiment and density-functional calculations, Phys. Rev. B 76, 155413 (2007)
S. Günther, S. Bocklein, R. Reichelt, J. Wintterlin, A. Barinov, T.O. Menteş, M.A. Niño, A. Locatelli: Surface patterning of silver using an electron- or photon-assisted oxidation reaction, ChemPhysChem 11, 1525–1532 (2010)
J. Laverock, S. Kittiwatanakul, A.A. Zakharov, Y.R. Niu, B. Chen, S.A. Wolf, J.W. Lu, K.E. Smith: Direct observation of decoupled structural and electronic transitions and an ambient pressure monocliniclike metallic phase of VO2, Phys. Rev. Lett. 113, 216402 (2014)
J. Laverock, S. Kittiwatanakul, A.A. Zakharov, Y.R. Niu, B. Chen, J. Kuyyalil, S.A. Wolf, J.W. Lu, K.E. Smith: Simultaneous spectroscopic, diffraction and microscopic study of the metal-insulator transition of VO2, MRS Proceedings 1730, Mrsf14-1730-n05-04 (2015)
F. Genuzio, A. Sala, T. Schmidt, D. Menzel, H.-J. Freund: Phase transformations in thin iron oxide films: Spectromicroscopic study of velocity and shape of the reaction fronts, Surf. Sci. 648, 177–187 (2016)
L.K.E. Ericsson, K.O. Magnusson, A.A. Zakharov: ZnO nanocrystals on SiO2/Si surfaces thermally cleaned in ultrahigh vacuum and characterized using spectroscopic photoemission and low energy electron microscopy, J. Vac. Sci. Technol. A 28, 438–442 (2010)
E. Bauer, K.L. Man, A. Pavlovska, A. Locatelli, T.O. Menteş, M.A. Niño, M.S. Altman: Fe3S4 (greigite) formation by vapor-solid reaction, J. Mater. Chem. A 2, 1903–1913 (2014)
K.L. Man, A. Pavlovska, E. Bauer, A. Locatelli, T.O. Menteş, M.A. Niño, G.K.L. Wong, I.K. Sou, M.S. Altman: Growth, reaction and nanowire formation of Fe on the ZnS(100) surface, J. Phys. Condens. Matter 26, 315006 (2014)
M. Ewert, T. Schmidt, J.I. Flege, I. Heidmann, T. Grzela, W.M. Klesse, M. Foerster, L. Aballe, T. Schroeder, J. Falta: Morphology and chemical composition of cobalt germanide islands on Ge(001), Nanotechnology 27, 325705 (2016)
M. Monti, B. Santos, A. Mascaraque, O.R. de la Fuente, M.A. Niño, T.O. Menteş, A. Locatelli, K.F. McCarty, J.F. Marco, J. de la Figuera: Oxidation pathways in bicomponent ultrathin iron oxide films, J. Phys. Chem. C 116, 11539–11547 (2012)
A. Cornish, T. Eralp, A. Shavorskiy, R.A. Bennett, G. Held, S.A. Cavill, A. Potenza, H. Marchetto, S.S. Dhesi: Oxidation of polycrystalline Ni studied by spectromicroscopy: Phase separation in the early stages of crystallite growth, Phys. Rev. B 81, 085403 (2010)
L. Aballe, S. Matencio, M. Foerster, E. Barrena, F. Sánchez, J. Fontcuberta, C. Ocal: Instability and surface potential modulation of self-patterned (001)SrTiO3 surfaces, Chem. Mater. 27, 6198–6204 (2015)
L. Aballe, A. Barinov, A. Locatelli, S. Heun, M. Kiskinova: Tuning surface reactivity via electron quantum confinement, Phys. Rev. Lett. 93, 196103 (2004)
L. Aballe, A. Barinov, N. Stojic, N. Binggeli, T.O. Menteş, A. Locatelli, M. Kiskinova: The electron density decay length effect on surface reactivity, J. Phys. Condens. Matter 22, 015001 (2010)
B. Kaemena, S.D. Senanayake, A. Meyer, J.T. Sadowski, J. Falta, J.I. Flege: Growth and morphology of ceria on ruthenium (0001), J. Phys. Chem. C 117, 221–232 (2013)
J.I. Flege, J. Höcker, B. Kaemena, T.O. Menteş, A. Sala, A. Locatelli, S. Gangopadhyay, J.T. Sadowski, S.D. Senanayake, J. Falta: Growth and characterization of epitaxially stabilized ceria(001) nanostructures on Ru(0001), Nanoscale 8, 10849–10856 (2016)
J. Höcker, T.O. Menteş, A. Sala, A. Locatelli, T. Schmidt, J. Falta, S.D. Senanayake, J.I. Flege: Unraveling the dynamic nanoscale reducibility (Ce4+ $$\rightarrow$$ Ce3+) of CeOx-Ru in hydrogen activation, Adv. Mater. Interfaces 2, 1500314 (2015)
J. Höcker, J.-O. Krisponeit, J. Cambeis, A. Zakharov, Y. Niu, G. Wei, L. Colombi Ciacchi, J. Falta, A. Schaefer, J.I. Flege: Growth and structure of ultrathin praseodymium oxide layers on ruthenium(0001), Phys. Chem. Chem. Phys. 19, 3480–3485 (2017)
D.C. Grinter, C.-M. Yim, C.L. Pang, B. Santos, T.O. Menteş, A. Locatelli, G. Thornton: Oxidation state imaging of ceria island growth on Re(0001), J. Phys. Chem. C 117, 16509–16514 (2013)
D.C. Grinter, C. Muryn, B. Santos, B.-J. Shaw, T.O. Menteş, A. Locatelli, G. Thornton: Spectromicroscopy of a model water–gas shift catalyst: Gold nanoparticles supported on ceria, J. Phys. Chem. C 118, 19194–19204 (2014)
D.C. Grinter, C. Muryn, A. Sala, C.-M. Yim, C.L. Pang, T.O. Menteş, A. Locatelli, G. Thornton: Spillover reoxidation of ceria nanoparticles, J. Phys. Chem. C 120, 11037–11044 (2016)
A. Locatelli, C. Sbraccia, S. Heun, S. Baroni, M. Kiskinova: Energetically driven reorganization of a modified catalytic surface under reaction conditions, J. Am. Chem. Soc. 127, 2351–2357 (2005)
A. Locatelli, T.O. Menteş, L. Aballe, A. Mikhailov, M. Kiskinova: Formation of regular surface-supported mesostructures with periodicity controlled by chemical reaction rate, J. Phys. Chem. B 110, 19108–19111 (2006)
A. Locatelli, L. Aballe, T.O. Menteş, F.Z. Guo, M. Kiskinova: A spectro-microscopic study of the reactive phase separation of Au\(+\)Pd and O on Rh(110), Surf. Sci. 601, 4663–4668 (2007)
F. Lovis, M. Hesse, A. Locatelli, T.O. Menteş, M.A. Nino, G. Lilienkamp, B. Borkenhagen, R. Imbihl: Self-organization of ultrathin vanadium oxide layers on a Rh(111) surface during a catalytic reaction. Part II: A LEEM and spectromicroscopy study, J. Phys. Chem. C 115, 19149–19157 (2011)
F. Lovis, T. Smolinsky, A. Locatelli, M.A. Niño, R. Imbihl: Chemical waves and rate oscillations in the H2\(+\) O2 reaction on a bimetallic Rh(111)/Ni catalyst, J. Phys. Chem. C 116, 4083–4090 (2012)
S. Günther, H. Liu, T.O. Menteş, A. Locatelli, R. Imbihl: Spectromicroscopy of pulses transporting alkali metal in a surface reaction, Phys. Chem. Chem. Phys. 15, 8752–8764 (2013)
S. Günther, S. Böcklein, J. Wintterlin, M.Á. Niño, T.O. Menteş, A. Locatelli: Locating catalytically active oxygen on Ag(111)—A spectromicroscopy study, ChemCatChem 5, 3342–3350 (2013)
A. Locatelli, C. Wang, C. Africh, N. Stojić, T.O. Menteş, G. Comelli, N. Binggeli: Temperature-driven reversible rippling and bonding of a graphene superlattice, ACS Nano 7, 6955–6963 (2013)
L.I. Johansson, S. Watcharinyanon, A.A. Zakharov, T. Iakimov, R. Yakimova, C. Virojanadara: Stacking of adjacent graphene layers grown on C-face SiC, Phys. Rev. B 84, 125405 (2011)
C. Coletti, S. Forti, A. Principi, K.V. Emtsev, A.A. Zakharov, K.M. Daniels, B.K. Daas, M.V.S. Chandrashekhar, T. Ouisse, D. Chaussende, A.H. MacDonald, M. Polini, U. Starke: Revealing the electronic band structure of trilayer graphene on SiC: An angle-resolved photoemission study, Phys. Rev. B 88, 155439 (2013)
M.S. Nevius, F. Wang, C. Mathieu, N. Barrett, A. Sala, T.O. Menteş, A. Locatelli, E.H. Conrad: The bottom-up growth of edge specific graphene nanoribbons, Nano Lett. 14, 6080–6086 (2014)
F. Wang, G. Liu, S. Rothwell, M.S. Nevius, C. Mathieu, N. Barrett, A. Sala, T.O. Menteş, A. Locatelli, P.I. Cohen, L.C. Feldman, E.H. Conrad: Pattern induced ordering of semiconducting graphene ribbons grown from nitrogen-seeded SiC, Carbon 82, 360–367 (2015)
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Bauer, E. (2019). LEEM, SPLEEM and SPELEEM. In: Hawkes, P.W., Spence, J.C.H. (eds) Springer Handbook of Microscopy. Springer Handbooks. Springer, Cham. https://doi.org/10.1007/978-3-030-00069-1_9
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