Electron Crystallography

  • Douglas L. Dorset
  • Sven Hovmöller
  • Xiaodong Zou

Part of the NATO ASI Series book series (NSSE, volume 347)

Table of contents

  1. Front Matter
    Pages i-xviii
  2. Background

  3. Experimental Techniques and Simulations

  4. Crystallographic Phase Determination

  5. Structure Refinement

About this book

Introduction

The re-emergent field of quantitative electron crystallography is described by some of its most eminent practitioners. They describe the theoretical framework for electron scattering, specimen preparation, experimental techniques for optimum data collection, the methodology of structure analysis and refinement, and a range of applications to inorganic materials (including minerals), linear polymers, small organic molecules (including those used in nonlinear optical devices), incommensurately modulated structures (including superconductors), alloys, and integral membrane proteins. The connection between electron crystallography and X-ray crystallography is clearly defined, especially in the utilisation of the latest methods for direct determination of crystallographic phases, as well as the unique role of image analysis of high-resolution electron micrographs for phase determination. Even the aspect of multiple beam dynamic diffraction (once dreaded because it was thought to preclude ab initio analysis) is considered as a beneficial aid for symmetry determination as well as the elucidation of crystallographic phases, and as a criterion for monitoring the progress of structure refinement. Whereas other texts have hitherto preferentially dealt with the analysis of electron diffraction and image data from thin organic materials, this work discusses - with considerable optimism - the prospects of looking at `harder' materials, composed of heavier atoms.
Audience: Could be used with profit as a graduate-level course on electron crystallography. Researchers in the area will find a statement of current progress in the field.

Keywords

X-ray crystallography crystal crystallography electron polymer scattering structure

Editors and affiliations

  • Douglas L. Dorset
    • 1
  • Sven Hovmöller
    • 2
  • Xiaodong Zou
    • 2
  1. 1.Electron Diffraction DepartmentHauptman-Woodward Medical Research Institute, Inc.BuffaloUSA
  2. 2.Structural ChemistryStockholm UniversityStockholmSweden

Bibliographic information

  • DOI https://doi.org/10.1007/978-94-015-8971-0
  • Copyright Information Springer Science+Business Media B.V. 1997
  • Publisher Name Springer, Dordrecht
  • eBook Packages Springer Book Archive
  • Print ISBN 978-90-481-4965-0
  • Online ISBN 978-94-015-8971-0
  • Series Print ISSN 0168-132X
  • About this book
Industry Sectors
Chemical Manufacturing