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Solid Sample Analysis

Direct and Slurry Sampling using GF-AAS and ETV-ICP

  • Book
  • © 1998

Overview

Editors:
  1. Ulrich Kurfürst

    1. Fachhochschule Fulda, Department of Nutrition, University of Applied Sciences, Fulda, Germany

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  • Written by an experienced practitioner for practitioners; book gives insight into the methodological and instrumental details enabling the practitioners to develop their own methods; extended chapters on qualitiy control and measurement uncertainty according to ISO.

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Table of contents (6 chapters)

  1. Front Matter

    Pages I-XIX
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  2. Characteristics of Solid Sampling Using the Graphite Furnace

    • Ulrich Kurfürst
    Pages 1-19

  3. General Aspects of the Graphite Furnace Solid Sampling Method

    • Ulrich Kurfürst
    Pages 21-127

  4. Direct Solid Sampling with Graphite Furnace Atomic Absorption Spectrometry (GF-AAS)

    • Ulrich Kurfürst
    Pages 129-190

  5. Solid Sampling by Electrothermal Vaporization-Inductively Coupled Plasma-Atomic Emission and -Mass Spectrometry (ETV-ICP-AES/-MS)

    • Peter Verrept, Sylvie Boonen, Luc Moens, Richard Dams
    Pages 191-246

  6. Introduction of Slurry Samples into the Graphite Furnace

    • Markus Stoeppler, Ulrich Kurfürst
    Pages 247-318

  7. Advantageous Fields of Application for Solid Sampling Analysis

    • Jürgen Fleckenstein, Markus Stoeppler, Ulrich Kurfürst
    Pages 319-388

  8. Back Matter

    Pages 389-427
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Keywords

About this book

The analysis of solid materials by introducing solid test sampies directly into the graphite furnace of an atomic absorption spectrometer must be regarded as a powerful analytical approach. Even if it is - of course - not the "ultimate method". After three decades of development, the instrumentation and the methodology are available to apply solid sampling successfully for the analysis of almost every material. Moreover, several tasks cannot be solved using other analytical methods as neatly as they can using direct solid sampling. The conventional methods work more or less satisfactorily, so why do we sug­ gest applying solid sampling much more extensively than it is today? To begin with, the features pointed out time and again should be named: Rapidity of the analytical procedure, low susceptibility to analyte loss or contamination, very smallquantities can be analyzed, and expenditure on instrumentation and per­ sonell is also low. These properties are examined and the necessary conditions are discussed (Chapter 1) as are the analytical tasks (Chapter 6) for which use of this method is advantageous. Other features that are often overlooked are just as important: The simplicity of the analytical procedures allows the analyst to main­ tain an intimate relationship with the original scientific task that has to be solved with the analysis. Furthermore, the considerable reduction of working place haz­ ards and pollution by avoiding the use of chemical reagents must nowadays be assessed as a feature as important as the others.

Editors and Affiliations

  • Fachhochschule Fulda, Department of Nutrition, University of Applied Sciences, Fulda, Germany

    Ulrich Kurfürst

Bibliographic Information

  • Book Title: Solid Sample Analysis

  • Book Subtitle: Direct and Slurry Sampling using GF-AAS and ETV-ICP

  • Editors: Ulrich Kurfürst

  • DOI: https://doi.org/10.1007/978-3-662-03716-4

  • Publisher: Springer Berlin, Heidelberg

  • eBook Packages: Springer Book Archive

  • Copyright Information: Springer-Verlag Berlin Heidelberg 1998

  • Hardcover ISBN: 978-3-540-62470-7Published: 18 March 1998

  • Softcover ISBN: 978-3-642-08290-0Published: 22 September 2011

  • eBook ISBN: 978-3-662-03716-4Published: 17 April 2013

  • Edition Number: 1

  • Number of Pages: XIX, 427

  • Number of Illustrations: 49 b/w illustrations

  • Topics: Analytical Chemistry

  • Industry Sectors: Biotechnology, Chemical Manufacturing, Pharma

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