Analytical Calorimetry

1. Front Matter

   Pages i-xii

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2. The Construction of a Microcalorimeter and Measurement of Heats of Solution of Stretched Glassy Polystyrene

   • Y. Takashima, K. Miasa, S. Miyata, K. Sakaoku

   Pages 1-6

3. Recent Advances in Titration Calorimetry

   • Lee D. Hansen, Reed M. Izatt, Delbert J. Eatough, Trescott E. Jensen, James J. Christensen

   Pages 7-16

4. Theory of Differential Scanning Calorimetry — Coupling of Electronic and Thermal Steps

   • Joseph H. Flynn

   Pages 17-44

5. On the Temperature Resolution of Thermistors

   • Peter W. Carr, Larry D. Bowers

   Pages 45-55

6. The Development and Application of an Ultra-Sensitive Quantitative Effluent Gas Analysis Technique

   • P. A. Barnes, E. Kirton

   Pages 57-67

7. A Small, Mini-Computer-Automated Thermoanalytical Laboratory

   • E. Catalano, J. C. English

   Pages 69-80

8. Steady State Technique for Low Temperature Heat Capacity of Small Samples

   • R. Viswanathan

   Pages 81-88

9. Fusion as an Opportunity for Calorimetrically Probing Polymer Conformations and Interactions in the Bulk State

   • Alan E. Tonelli

   Pages 89-101

10. Application of Differential Scanning Calorimetry for the Study of Phase Transitions

    • William P. Brennan

    Pages 103-117

11. Importance of Joint Knowledge of ΔH° and ΔS° Values for Interpreting Coordination Reactions in Solution

    • Guy Berthon

    Pages 119-125

12. The Determination of the Heat of Fusion by Differential Scanning Calorimetry and by Measurements of the Heat of Dissolution

    • Erwin E. Marti

    Pages 127-135

13. Novel Methods for Gas Generating Reactions

    • Allen A. Duswalt

    Pages 137-146

14. DSC: New Developments in Clinical Analysis and Physiochemical Research

    • Bruce Cassel, Tsuyoshi Ohnishi

    Pages 147-163

15. The Use of Thermal and Ultrasonic Data to Calculate the Pressure Dependence of the Gruneisen Parameter

    • S. R. Urzendowski, A. H. Guenther

    Pages 165-184

16. The Use of Thermal Evolution Analysis (TEA) for the Determination of Vapor Pressure of Agricultural Chemicals

    • Roger L. Blaine, Paul F. Levy

    Pages 185-198

17. Thermal Evolution Analysis of Some Organic Materials

    • Edward W. Kifer, Lee H. Leiner

    Pages 199-205

18. High Sensitivity Enthalpimetric Determination of Olefins

    • L. A. Williams, B. Howard, D. W. Rogers

    Pages 207-216

19. Biochemical and Clinical Applications of Titration Calorimetry and Enthalpimetric Analysis

    • Albert C. Censullo, John A. Lynch, Dan H. Waugh, Joseph Jordan

    Pages 217-235

20. Recent Analytical Applications of Titration Calorimetry

    • Reed M. Izatt, Lee D. Hansen, Delbert J. Eatough, Trescott E. Jensen, James J. Christensen

    Pages 237-248

The research reported in the third volume of Analytical Calorimetry covers a wide variety of topics. The variety indicates the sophistication which thermal analysis is reaching and addition­ ally the ever widening applications that are being developed, Advances in instrumentation include: microcalorimeter design, development and refinement of titration calorimetry, definition of further theory of scanning calorimetry, studies of the temperature of resolution of thermistors, and a refinement of the effluent gas analysis technique and its application to agricultural chemicals as well as organic materials. A wide variety of applications is reported. These cover the fields of polymeric materials, dental materials, inorganic proteins, biochemical materials, gels, mixed crystals, and other specialized areas. Contributions also include applications of important related techniques such as thermomechanical and thermogravimetric analysis. The contributions to this Volume represent papers presented before the Division of Analytical Chemistry at the Third Symposium on Analytical Chemistry held at the 167th National Meeting of the American Chemical Society, March 30 - April 5, 1974.

• Atom
• agriculture
• analytical chemistry
• bonding
• calorimeter
• chemical reaction
• chemistry
• development
• enthalpy
• fields
• kinetics
• metals
• paper
• society
• thermodynamics

• Polymer Science and Engineering, University of Massachusetts, Amherst, USA

  Roger S. Porter

• Department of Chemistry and Institute of Materials Science, University of Connecticut, Storrs, USA

  Julian F. Johnson

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