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The Multinuclear Approach to NMR Spectroscopy

  • Joseph B. Lambert
  • Frank G. Riddell

Part of the NATO ASI Series book series (ASIC, volume 103)

Table of contents

  1. Front Matter
    Pages i-xvi
  2. G. A. Webb
    Pages 49-61
  3. Joseph B. Lambert
    Pages 91-110
  4. K. J. Packer
    Pages 111-131
  5. Harold C. Jarrell, Ian C. P. Smith
    Pages 133-149
  6. Harold C. Jarrell, Ian C. P. Smith
    Pages 151-168
  7. Robert L. Lichter
    Pages 207-244
  8. Pierre Laszlo
    Pages 261-296
  9. Otto Lutz
    Pages 297-308
  10. Torbjörn Drakenberg, Sture Forsén
    Pages 309-328
  11. R. Garth Kidd
    Pages 329-341
  12. Otto Lutz
    Pages 389-403
  13. Torbjörn Drakenberg, Sture Forsén
    Pages 405-444
  14. R. Garth Kidd
    Pages 445-456
  15. Back Matter
    Pages 525-548

About this book

Introduction

The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene­ fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech­ niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan­ tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.

Keywords

field nuclear magnetic resonance (NMR) spectroscopy

Editors and affiliations

  • Joseph B. Lambert
    • 1
  • Frank G. Riddell
    • 2
  1. 1.Department of ChemistryNorthwestern UniversityEvanstonUSA
  2. 2.Department of ChemistryUniversity of StirlingStirlingScotland

Bibliographic information

  • DOI https://doi.org/10.1007/978-94-009-7130-1
  • Copyright Information Springer Science+Business Media B.V. 1983
  • Publisher Name Springer, Dordrecht
  • eBook Packages Springer Book Archive
  • Print ISBN 978-94-009-7132-5
  • Online ISBN 978-94-009-7130-1
  • Series Print ISSN 1389-2185
  • Buy this book on publisher's site
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