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NMR — From Spectra to Structures

An Experimental Approach

  • Terence N. Mitchell
  • Burkhard Costisella

Table of contents

  1. Front Matter
    Pages I-XIII
  2. Introduction

    1. Pages 1-2
  3. NMR Experiments

    1. Pages 3-39
    2. Pages 39-51
    3. Pages 53-59
    4. Pages 59-72
    5. Pages 73-83
    6. Back Matter
      Pages 84-84
  4. Worked Example and Problems

    1. Pages 85-88
    2. Pages 88-91
    3. Pages 93-163
    4. Pages 164-207

About this book

Introduction

Nuclear magnetic resonance spectroscopy is one of the most powerful analytical methods. This practice-oriented textbook aims at teaching how NMR experiments should be used to make structural asssignments. The book is intended as a practical guide for students and laboratory personnel, so that the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results.
The second edition has been expanded to include several other heteronuclei (15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb) and a new chapter on solid state NMR. The problems section has been enlarged and now includes 50 problems. These are of different degrees of complexity and in all cases include two-dimensional (2D) methods as well as standard proton and carbon 1D spectra.

Keywords

Experiment NMR nuclear magnetic resonance programmable logic controller spectroscopy structure determination structure elucidation

Authors and affiliations

  • Terence N. Mitchell
    • 1
  • Burkhard Costisella
    • 1
  1. 1.Fachbereich ChemieUniversität DortmundDortmundGermany

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