Skip to main content

Advertisement

SpringerLink
Log in

Visual spectroscopy detection of triclosan

  • Short Communication
  • Published:
Chemical Papers Aims and scope Submit manuscript

Abstract

The azo coupling reaction with 2-aminonaphthalene-4,8-disulfonic acid (I) was used to develop a new cheap and rapid method of triclosan (II) determination in hygiene products. The calibration graph was linear in the range of 2.0−100 × 10−6 mol L−1. The detection limit was 2.0 μmol L−1.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

References

  • Agronomov, A. E. (1990). Chosen chapters of organic chemistry. Moscow, Russia: Khimiya. (in Russian)

    Google Scholar 

  • Amiri, M., Shahrokhian, S., Psillakis, E., & Marken, F. (2007). Electrostatic accumulation and determination of triclosan in ultrathin carbon nanoparticle composite film electrodes. Analytica Chimica Acta, 593, 117–122. DOI: 10.1016/j.aca.2007.04.042.

    Article  CAS  Google Scholar 

  • Canosa, P., Pérez-Palacios, D., Garrido-López, A., Tena, M. T., Rodríguez, I., Rubí, E., & Cela, R. (2007a). Pressurized liquid extraction with in-cell clean-up followed by gas chromatography-tandem mass spectrometry for the selective determination of parabens and triclosan in indoor dust. Journal of Chromatography A, 1161, 105–112. DOI: 10.1016/j.chroma.2007.05.089.

    Article  CAS  Google Scholar 

  • Canosa, P., Rodríguez, I., Rubí, E., & Cela, R. (2007b). Determination of parabens and triclosan in indoor dust using matrix solid-phase dispersion and gas chromatography with tandem mass spectrometry. Analytical Chemistry, 79, 1675–1681. DOI: 10.1021/ac061896e.

    Article  CAS  Google Scholar 

  • Canosa, P., Rodríguez, I., Rubí, E., Ramil, M., & Cela, R. (2008). Simplified sample preparation method for triclosan and methyltriclosan determination in biota and foodstuff samples. Journal of Chromatography A, 1188, 132–139. DOI: 10.1016/j.chroma.2008.02.064.

    Article  CAS  Google Scholar 

  • Chu, S., & Metcalfe, C. D. (2007). Simultaneous determination of triclocarban and triclosan in municipal biosolids by liquid chromatography tandem mass spectrometry. Journal of Chromatography A, 1164, 212–218. DOI: 10.1016/j.chroma.2007.07.024.

    Article  CAS  Google Scholar 

  • Gatidou, G., Thomaidis, N. S., Stasinakis, A. S., & Lekkas, T. D. (2007). Simultaneous determination of the endocrine disrupting compounds nonylphenol, nonylphenol ethoxylates, triclosan and bisphenol A in wastewater and sewage sludge by gas chromatography-mass spectrometry. Journal of Chromatography A, 1138, 32–41. DOI: 10.1016/j.chroma.2006.10.037.

    Article  CAS  Google Scholar 

  • Lu, H., Ma, H., & Tao, G. (2009). Spectrophotometric determination of triclosan in personal care products. Spectrochimica Acta Part A, 73, 854–857. DOI: 10.1016/j.saa.2009.04.007.

    Article  Google Scholar 

  • Lur’e, Y. Y. (1989). Handbook of analytical chemistry. Moscow, Russia: Khimiya. (in Russian)

    Google Scholar 

  • Morales, S., Canosa, P., Rodríguez, I., Rubí, E., & Cela, R. (2005). Microwave assisted extraction followed by gas chromatography with tandem mass spectrometry for the determination of triclosan and two related chlorophenols in sludge and sediments. Journal of Chromatography A, 1082, 128–135. DOI: 10.1016/j.chroma.2005.05.059.

    Article  CAS  Google Scholar 

  • Quintana, J. B., & Reemtsma, T. (2004). Sensitive determination of acidic drugs and triclosan in surface and wastewater by ion-pair reverse-phase liquid chromatography/tandem mass spectrometry. Rapid Communications in Mass Spectrometry, 18, 765–774. DOI: 10.1002/rcm.1403.

    Article  CAS  Google Scholar 

  • Rule, K. L., Ebbett, V. R., & Vikesland, P. J. (2005). Formation of chloroform and chlorinated organics by free-chlorinemediated oxidation of triclosan. Environmental Science & Technology, 39, 3176–3185. DOI: 10.1021/es048943+.

    Article  CAS  Google Scholar 

  • Serjeant, E. P., & Dempsey, B. (1979). Ionisation constants of organic acids in aqueous solution. Oxford, UK: Pergamon Press.

    Google Scholar 

  • Song, S., Song, Q. J., & Chen, Z. (2007). Online phototransformation-flow injection chemiluminescence determination of triclosan. Analytical and Bioanalytical Chemistry, 387, 2917–2922. DOI: 10.1007/s00216-007-1130-5.

    Article  CAS  Google Scholar 

  • Whitlock, L. R., Siggia, S., & Smola, J. E. (1972). Spectrophotometric analysis of phenols and of sulfonates by formation of an azo dye. Analytical Chemistry, 44, 532–536. DOI: 10.1021/ac60311a021.

    Article  CAS  Google Scholar 

  • Zaporozhets, O. A., Nadzhafova, O. Y., Verba, V. V., Sukhan, V. V., Dolenko, S. A., & Keda, T. Y. (1998). Solid-phase reagents for the determination of anionic surfactants in water. Analyst, 123, 1583–1586. DOI: 10.1039/a708811f.

    Article  CAS  Google Scholar 

  • Zaporozhets, O. A., Zin’ko, L. S., & Kachan, I. A. (2007). Solidphase-spectrophotometric and test determination of simultaneously present phosphorus forms (phosphorus speciation) in water. Journal of Analytical Chemistry, 62, 1146–1150. DOI: 10.1134/S1061934807120088.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Analytical Chemistry, Taras Shevchenko National University of Kyiv, 64 Volodymyrska str., 01033, Kyiv, Ukraine

    Olexander I. Kysliak & Natalia I. Smyk

Authors
  1. Olexander I. Kysliak
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Natalia I. Smyk
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Olexander I. Kysliak.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Kysliak, O.I., Smyk, N.I. Visual spectroscopy detection of triclosan. Chem. Pap. 64, 523–527 (2010). https://doi.org/10.2478/s11696-010-0026-6

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.2478/s11696-010-0026-6

Keywords

Search

Navigation