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Determination of lead in solution by solid phase extraction, elution, and spectrophotometric detection using 4-(2-pyridylazo)-resorcinol

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Central European Journal of Chemistry

Abstract

Lead (+2) was selectively adsorbed on a solid phase extraction (SPE) gel (molecular recognition technology, MRT), quantitatively extracted, and spectrophotometrically determined as the Pb(II)-PAR (4-(2-pyridylazo)-resorcinol) complex. The linear range was 0.01 to 0.75 mg L−1 and the detection limit was 6.4 µg L−1. The MRT-SPE allows selective Pb(II) extraction from complex ion-rich matrices, which is difficult with other techniques. Interference from common matrix ions such as Fe2+, Ni2+, Cu2+ or Co2+ is minimized.

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Authors and Affiliations

  1. Graduate School of Natural Science and Technology, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan

    Ismail M. M. Rahman & Zinnat A. Begum

  2. Department of Applied and Environmental Chemistry, University of Chittagong, Chittagong, 4331, Bangladesh

    Ismail M. M. Rahman

  3. GL Sciences Inc., Nishishinjuku 6-22-1, Shinjuku, Tokyo, 163-1130, Japan

    Yoshiaki Furusho

  4. Kyoritsu Chemical Check Lab., Corp., Ohta-ku, Tokyo, 145-0071, Japan

    Rika Sato, Hiroshi Okumura & Hiroko Honda

  5. Institute of Science and Engineering, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan

    Hiroshi Hasegawa

Authors
  1. Ismail M. M. Rahman
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  2. Yoshiaki Furusho
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  3. Zinnat A. Begum
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  4. Rika Sato
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  5. Hiroshi Okumura
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  7. Hiroshi Hasegawa
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Correspondence to Ismail M. M. Rahman.

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Rahman, I.M.M., Furusho, Y., Begum, Z.A. et al. Determination of lead in solution by solid phase extraction, elution, and spectrophotometric detection using 4-(2-pyridylazo)-resorcinol. cent.eur.j.chem. 11, 672–678 (2013). https://doi.org/10.2478/s11532-013-0203-x

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  • DOI: https://doi.org/10.2478/s11532-013-0203-x

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