Preparation of Centimeter-Sized Zeolite Crystals by Hydrothermal Seeded Growth

Abstract

Centimeter-sized crystals of pyridine dodecasil 3C (all silica zeolite ZSM-39) have been prepared using hydrothermal seeded growth techniques and characterized by differential scanning calorimetry, nuclear magnetic resonance, optical microscopy and powder X-ray diffraction.

This is a preview of subscription content, access via your institution.

References

  1. 1.

    G. A. Ozin, A. Kuperman, A. Stein, Angew. Chem. Int. Ed. Engl. 28, 359 (1989).

    Article  Google Scholar 

  2. 2.

    A. Kuperman, S. Nadimi, S. Oliver, G. A. Ozin, J. M. Garces, M. M. Olken, Nature 365, 239 (1993), and references cited therein.

    CAS  Article  Google Scholar 

  3. 3.

    H. Gies, F. Liebau, H. Gerke, Angew. Chem. Int. Ed. Engl. 21, 206 (1982).

    Article  Google Scholar 

  4. 4.

    J. L. Schlenker, F. G. Dwyer, E. E. Jenkins, W. J. Rohrbaugh, G. T. Kokotailo, W. M. Meier, Nature 294, 340 (1981).

    CAS  Article  Google Scholar 

  5. 5.

    W. M. Meier, D. H. Olson. Atlas of Zeolite Structure Types (Butterworths: London,1987) pp. 104–105.

    Google Scholar 

  6. 6.

    H. K. Chae, W. G. Klemperer, D. A. Payne, C. T. A. Suchicital, D. R. Wake, S. R. Wilson in Materials for Nonlinear Optics: Chemical Perspectives, edited by S. R. Marder, J. E. Sohn and G. D. Stucky (Am. Chem. Soc. Sym. Series 455, Boston, MA, 1991) pp. 528–540.

  7. 7.

    H. Gies in Inclusion Compounds, Volume 5, Inorganic and Physical Aspects of Inclusion, edited by J. L. Atwood, J. E. D. Davies and D. D. MacNicol (Oxford University Press, Oxford, 1991) pp. 1–36.

  8. 8.

    R. A. Laudise, R. L. Barns, IEEE Transactions on Ultrasonics, Ferroelectrics, and Frequency Control 35 277 (1988).

    CAS  Article  Google Scholar 

  9. 9.

    H. K. Chae, W. G. Klemperer, D. A. Payne, C. T. A. Suchicital, in IEEE Int. Symp. Appl. Ferroelectr. 7th 491 (1991).

    Google Scholar 

  10. 10.

    J. A. Ripmeester, M. A. Desando, Y. P. Handa, J. S. Tse, J. Chem. Soc, Chem. Commun. 608 (1988).

    Google Scholar 

  11. 11.

    J. S. Tse, M. Desando, J. A. Ripmeester, Y. P. Handa, J. Am. Chem. Soc. 115, 281 (1993).

    CAS  Article  Google Scholar 

Download references

Author information

Affiliations

Authors

Corresponding author

Correspondence to Walter G. Klemperer.

Rights and permissions

Reprints and Permissions

About this article

Cite this article

Klemperer, W.G., Marquart, T.A. Preparation of Centimeter-Sized Zeolite Crystals by Hydrothermal Seeded Growth. MRS Online Proceedings Library 346, 819–824 (1994). https://doi.org/10.1557/PROC-346-819

Download citation