Abstract
A comparison of microcompression and microtensile methods to study mechanical properties of electrodeposited nanocrystalline (nc) nickel has been performed. Microtensile tests that probe a volume of more than 2 × 106 μm3 show reasonable agreement with results from microcompression tests that probe much smaller volumes down to a few μm3. Differences between the two uniaxial techniques are discussed in terms of measurements errors, probed volume and surface effects, strain rate, and influence of stress state. Uniaxial solicitation in compression mode revealed several advantages for studying stress–strain properties.
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References
- 1
Y. Yang, B.I. Imasogie, S.M. Allameh, B. Boyce, K. Lian, J. Lou W.O. Soboyejo: Mechanisms of fatigue in LIGA Ni MEMS thin films. Mater. Sci. Eng., A 444, 39 2007
- 2
B. Li Q. Chen: Solid micromechanical valves fabricated with in situ UV-LIGA assembled nickel. Sens. Actuators, A 126, 187 2006
- 3
N.R. Moody, J.M. Jungk, M.S. Kennedy, S.V. Prasad, D.F. Bahr W.W. Gerberich: Mechanical properties of wear tested LIGA nickel in Fundamentals of Nanoindentation and Nanotribology III, edited by K.J. Wahl, N. Huber, A.B. Mann, D.F. Bahr, and Y-T. Cheng (Mater. Res. Soc. Symp. Proc. 841 Warrendale, PA, 2005), R7.8
- 4
K.S. Kumar, H. Van Swygenhoven S. Suresh: Mechanical behaviour of nanocrystalline metals and alloys. Acta Mater. 51, 5743 2003
- 5
W.D. Nix, J.R. Greer, G. Feng E.T. Lilleodden: Deformation at the nanometer and micrometer length scales: Effects of strain gradients and dislocation starvation. Thin Solid Films 515, 3152 2007
- 6
E. Mazza, S. Abel J. Dual: Experimental determination of mechanical properties of Ni and Ni–Fe microbars. Microsyst. Technol. 2, 197 1996
- 7
M.A. Haque M.T.A. Saif: In-situ tensile testing of nanoscale specimens in SEM and TEM. Exp. Mech. 42(1), 123128 2001
- 8
B. Moser, R. Schwaiger M. Dao: Size effects on deformation and fracture on nanostructured materials in Nanostructured Coating, edited by A. Cavaleiro and J.Th.M. De Hosson, Nanostructure Science and Technology Series Springer, New York} 2
- 9
J.R. Greer, W.C. Oliver W.D. Nix: Size dependence of mechanical properties of gold at the micron scale in the absence of strain gradients. Acta Mater. 53, 1821 2005
- 10
M.D. Uchic, D.M. Dimiduk, J.N. Florando W.D. Nix: Sample dimensions influence strength and crystal plasticity. Science 305, 986 2004
- 11
H.D. Espinosa, M. Panico, S. Berbenni K.W. Schwartz: Discrete dislocation dynamics simulations to interpret plasticity size and surface effects in freestanding fcc thin films. Int. J. Plast. 22, 2091 2006
- 12
W.D. Nix H. Gao: Indentation size effects in crystalline materials: a law for strain gradient plasticity. J. Mech. Phys. Solids 46, 411 1998
- 13
I.N. Sneddon: The relation between load and penetration in the axisymmetric Boussineq for a punch of arbitrary profile. Int. J. Eng. Sci. 3, 47 1965
- 14
H. Bei, S. Shim, M.K. Miller, G.R. Pharr E.P. George: Effects of focused-ion-beam milling on the nanomechanical behavior of a molybdenum-alloy single crystal. APL 91, 111915 2007
- 15
B. Moser, K. Wasmer, L. Barbieri J. Michler: Strength and fracture of Si micropillars: A new scanning electron microscopy-based micro-compression test. J. Mater. Res. 22(4), 1004 2007
- 16
H. Zhang, B.E. Schuster, Q. Wie K.T. Ramesh: The design of accurate micro-compression experiments. Scripta Mater. 54, 181 2006
- 17
W.F. Mohamad, A. Abou Ajar A.N. Saleh: Effects of oxide layers and metals on photoelectric and optical properties of Schottky barrier photodetector. Renew. Ener. 31, 1493 2006
- 18
R.J. Asaro S. Suresh: Mechanistic models for the activation volume and rate sensitivity in metals with nanocrystalline grains and nano-scale twins. Acta Mater. 53, 3369 2005
- 19
V.L. Tellkamp, A. Melmed E.J. Lavernia: Grain growth behavior of a nanostructured 5083 Al–Mg alloy. Metal. Mater. Trans. A 32, 2335 2001
- 20
T. Hanlon, Y-N. Kwon S. Suresh: Grain size effects on the fatigue response of nanocrystalline metals. Scripta Mater. 49, 675 2003
- 21
S. Cheng, J.A. Spencer W.W. Milligan: Strength and tension/compression asymmetry in nanostructured and ultrafine-grain metals. Acta Mater. 51, 4505 2003
- 22
J.L. Loubet, M. Bauer, A. Tonck, S. Bec B. Gauthier-Manuel: Mechanical Properties and Deformation Behaviour of Materials Having Ultra-fine Microstructures Kluwer Academic Publishers The Netherlands 1993 429–447
- 23
T. Chudoba, P. Schwaller, R. Rabe, J-M. Breguet J. Michler: Comparison of nanoindentation results obtained with Berkovich and cube-corner indenters. Philos. Mag. 86(33–35), 5265 2006
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Philippe, L., Schwaller, P., Bürki, G. et al. A comparison of microtensile and microcompression methods for studying plastic properties of nanocrystalline electrodeposited nickel at different length scales. Journal of Materials Research 23, 1383–1388 (2008). https://doi.org/10.1557/JMR.2008.0162
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