Abstract
The effect of chemical etching on the surface roughness and fracture strength of Nd:yttrium-aluminum-garnet single crystals was investigated. Etching the laser host material in a 1:1 mixture of concentrated sulfuric and phosphoric acid at elevated temperatures enabled material removal from the surface of laser rods cored from single-crystal boules. The roughness on the rod surface increased from the as-drilled condition after etching, but after 17 μm of material was removed, the roughness remained approximately constant. The modulus of rupture increased from 133-530 MPa when 87 μm of material was removed by the chemical etching procedure.
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References
- 1.
Q. Xiao and J. Derby. J. Crystal Growth 139, 147 (1994).
- 2.
S.M. Vatnik, R El-Agmy, and T. Graf, J. Mod. Optics 49, 2059 (2002).
- 3.
W.A. Clarkson, J. Phys. D: Appl. Phys. 34, 2381 (2001).
- 4.
W. Xie, S. Tam, Y. Lam, H. Yang, J. Liu, J. Gu, and W. Tan, Optics Laser Technol. 32, 193 (2003).
- 5.
W. Koechner, Solid State Laser Engineering, 5th ed. (Springer, Berlin, 1999), pp. 48, 406–413.
- 6.
T. Mah and T.A. Parthasarathy, Scripta Metall. Mater. 28, 1383 (1993).
- 7.
W.R. Blumenthal and S.T. Taylor, Acta Mater. 45, 3071 (1997).
- 8.
ASTM. ASTM Standard Test Methods for Strength of Glass by Flexure, Determination of Modulus of Rupture, Designation C 158 – 95 (ASTM, West Conshohocken, NJ, 1995).
- 9.
M. Gerber and Th. Graf, Optics Laser Technol. 33, 449 (2001).
- 10.
W. Koechner, Appl. Phys. 2, 279 (1973).
- 11.
F.L. Vogel, W.G. Pfann, H.E. Corey, and E.E. Thomas, Phys. Rev. 90, 489 (1953).
- 12.
A.T. Zlatkin and E.L. Lube, J. Crystal Growth 118, 218 (1992).
- 13.
J. Marion, Appl. Phys. Lett. 47, 694 (1985).
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Shafer, K.E., Eakins, D.E., Bahr, D.F. et al. Strength enhancement of single crystal laser components. Journal of Materials Research 18, 2537–2539 (2003). https://doi.org/10.1557/JMR.2003.0353
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