Abstract
Powders with a nanostructured mixture of pure Al and Pb phase were produced by mechanical milling of elemental blends of Al and Pb with a composition of Al90Pb10 (wt. %). Under a pressure of 1.5 GPa at 280 °C, the as-milled powders were successfully consolidated into bulk, full-density samples (>99.5% theoretical density) while the average grain sizes of Al and Pb in the compacted samples remain unchanged with respect to those in the as-milled powders. The achievement of the full density without grain coarsening in the consolidation process could be reasonably attributed to melting of the nanometer-sized Pb particles of which the melting point is considerably depressed.
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References
G. W. Nieman, J. R. Weertman, and R. W. Siegel, J. Mater. Res. 6, 1012 (1991).
R. W. Siegel and G. E. Fougere, in Nanophase Materials: Synthesis-Properties-Applications, edited by G. C. Hadjipanayis and R. W. Siegel (Kluwer, Dordrecht, 1994), p. 233.
K. Lu, Mater. Sci. Eng. Rep. 16, 161 (1996).
U. Erb, A. M. El-Sherik, G. Palumbo, and K. T. Aust, Nanostruc. Mater. 2, 383 (1993).
R. Z. Valiev, A. V. Korznikov, and R. P. Mulyukov, Mater. Sci. Eng. A168, 141 (1993).
M. Jain and T. Christman, Acta Metall. 42, 1901 (1994).
D. A. Morris and M. A. Morris, Acta Metall. Mater. 39, 1763 (1991).
M. Oehring, F. Appel, Th. Pfullmann, and R. Bormann, Appl. Phys. Lett. 66, 941 (1995).
C. Suryanarayana, G. E. Korth, and F. H. Froes, in Processing and Properties of Nanocrystalline Materials, edited by C. Suryanarayana, J. Singh, and F. H. Froes (The Minerals, Metals & Materials Society, Warrendale, PA, 1996), p. 291.
R. Suryanarayanan, C. A. Frey, and S. M. L. Sastry, J. Mater. Res. 11, 439 (1996).
L. He and E. Ma, J. Mater. Res. 11, 72 (1996).
K. N. P. Kumar, K. Keizer, A. J. Burggraaf, T. Okubo, H. Nagamoto, and S. Morooka, Nature (London) 358, 48 (1992).
H. W. Sheng, G. Ren, L. M. Peng, Z. H. Hu, and K. Lu, Philos. Mag. Lett. 73, 179 (1996).
H. W. Sheng, F. Zhou, Z. Q. Hu, and K. Lu, J. Mater. Res. 13, 308 (1998).
D. Nath, R. Bolla, and S. Chandra, Powder Met. Int. 24, 84 (1992).
H. W. Sheng, Z. Q. Hu, and K. Lu, Nanostruc. Mater. 9 661 (1997); H. W. Sheng, G. Ren, L. M. Peng, Z. Q. Hu, and K. Lu (unpublished).
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Zhou, F., Sheng, H.W. & Lu, K. Fully dense Al–Pb nanocomposite bulk samples consolidated from mechanically milled powders. Journal of Materials Research 13, 249–252 (1998). https://doi.org/10.1557/JMR.1998.0033
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DOI: https://doi.org/10.1557/JMR.1998.0033