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Synthesis of Laurylchitosan and Its Use in the Separation of Flavonoids from Aleurites moluccana by Matrix Solid-Phase Dispersion

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Abstract

Chitosan was modified with lauroyl chloride to prepare a solid support for the application of matrix solid-phase dispersion (MSPD) for the extraction of flavonoids from the medicinal plant Aleurites moluccana. The laurylchitosan prepared by the homogenous and heterogeneous method, was characterized using analytical methods such as potentiometric titration and infrared spectroscopy. The hydrophobic properties were studied by naphthalene incorporation. The MSPD performance was evaluated by extraction of swertisin and 2″-O-rhamnosylswertisin from the leaves of A. moluccana.

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Acknowledgment

This work was supported by grants from CNPq, ProBIC/ProPPEC/UNIVALI, FAPESC.

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Authors and Affiliations

  1. Núcleo de Investigações Químico-Farmacêuticas (NIQFAR), Universidade do Vale do Itajaí (UNIVALI), Itajai, Santa Catarina, 88302-202, Brazil

    Fernanda Cristina Stenger, Valdir Cechinel-Filho, Christiane Meyre-Silva, Tania Mari Belle Bresolin & Clóvis Antonio Rodrigues

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  1. Fernanda Cristina Stenger
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  2. Valdir Cechinel-Filho
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  3. Christiane Meyre-Silva
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  4. Tania Mari Belle Bresolin
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  5. Clóvis Antonio Rodrigues
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Corresponding author

Correspondence to Clóvis Antonio Rodrigues.

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Separation Analysis Applied to Pharmaceutical Sciences in Brazil.

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Stenger, F.C., Cechinel-Filho, V., Meyre-Silva, C. et al. Synthesis of Laurylchitosan and Its Use in the Separation of Flavonoids from Aleurites moluccana by Matrix Solid-Phase Dispersion. Chroma 69 (Suppl 2), 183–187 (2009). https://doi.org/10.1365/s10337-009-1016-0

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