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Chromatographia

, Volume 69, Supplement 2, pp 183–187 | Cite as

Synthesis of Laurylchitosan and Its Use in the Separation of Flavonoids from Aleurites moluccana by Matrix Solid-Phase Dispersion

  • Fernanda Cristina Stenger
  • Valdir Cechinel-Filho
  • Christiane Meyre-Silva
  • Tania Mari Belle Bresolin
  • Clóvis Antonio Rodrigues
Original

Abstract

Chitosan was modified with lauroyl chloride to prepare a solid support for the application of matrix solid-phase dispersion (MSPD) for the extraction of flavonoids from the medicinal plant Aleurites moluccana. The laurylchitosan prepared by the homogenous and heterogeneous method, was characterized using analytical methods such as potentiometric titration and infrared spectroscopy. The hydrophobic properties were studied by naphthalene incorporation. The MSPD performance was evaluated by extraction of swertisin and 2″-O-rhamnosylswertisin from the leaves of A. moluccana.

Keywords

Hydrophobicity Laurylchitosan Matrix solid-phase dispersion 

Notes

Acknowledgment

This work was supported by grants from CNPq, ProBIC/ProPPEC/UNIVALI, FAPESC.

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Copyright information

© Vieweg+Teubner | GWV Fachverlage GmbH 2009

Authors and Affiliations

  • Fernanda Cristina Stenger
    • 1
  • Valdir Cechinel-Filho
    • 1
  • Christiane Meyre-Silva
    • 1
  • Tania Mari Belle Bresolin
    • 1
  • Clóvis Antonio Rodrigues
    • 1
  1. 1.Núcleo de Investigações Químico-Farmacêuticas (NIQFAR)Universidade do Vale do Itajaí (UNIVALI)ItajaiBrazil

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