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Thermally Stimulated Evolution of the Surface of Ni- and Cu-Containing Plasma-Electrolytic Oxide Coatings on Titanium

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Abstract

The effect of the temperature of annealing in air on the surface architecture and composition of oxide layers has been studied. Copper-enriched nanosized crystals of triangular shape are present on the surface at the annealing temperatures of 500–700°С. Rectangular nano- and microcrystals of a possible composition of NiWO4 are formed on the surface after annealing at 750–850°С. Nanowhisker brushes, similar in composition to nickel titanates, cover the surface after annealing at 900–950°С. Transformation of the surface architecture and composition on the micro- and nanolevels correlates to the coatings’ activity in the catalysis of the reaction of oxidation of CO to CO2.

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FUNDING

The present work was partially supported by grant from the Russian Foundation for Basic Research no. 18-03-00418.

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Authors and Affiliations

  1. Institute of Chemistry, Far East Branch, Russian Academy of Sciences, 690022, Vladivostok, Russia

    V. S. Rudnev, I. V. Lukiyanchuk, M. S. Vasilyeva & A. A. Zvereva

  2. Far Eastern Federal University, 690091, Vladivostok, Russia

    V. S. Rudnev & M. S. Vasilyeva

Authors
  1. V. S. Rudnev
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  2. I. V. Lukiyanchuk
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  3. M. S. Vasilyeva
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  4. A. A. Zvereva
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Correspondence to V. S. Rudnev.

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Translated by D. Marinin

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Rudnev, V.S., Lukiyanchuk, I.V., Vasilyeva, M.S. et al. Thermally Stimulated Evolution of the Surface of Ni- and Cu-Containing Plasma-Electrolytic Oxide Coatings on Titanium. Prot Met Phys Chem Surf 55, 719–728 (2019). https://doi.org/10.1134/S2070205119040178

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  • DOI: https://doi.org/10.1134/S2070205119040178

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