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Structural Phase State and Thermal Cyclic Stability of the Thermal Barrier Zr–Si–O Coatings Deposited on a Copper Substrate by the Microplasma Method

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Abstract

In this work, preparation of thermal barrier coatings based on zirconium oxide is shown. The phased treatment of the copper substrate is proposed in order to obtain a layered thermal barrier oxide coating on it. The sample surface is nanostructured, titanium is deposited layer-by-layer (by the vacuum-arc method) and then zirconium (by the magnetron method), and then zirconium is converted into zirconium dioxide by the microplasma method. The formed oxide-ceramic coatings contain elements from a solution, according to the results of elemental analysis, and zirconium dioxide in tetragonal and monoclinic modifications, according to the results of X-ray diffraction. A study of thermal cyclic stability was carried out. It is revealed that an increase in the time of microplasma treatment to a certain value has a positive effect on the thermal cyclic properties of the obtained layer material and it is able to sustain more than 90 cycles without serious damage to the surface layer.

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FUNDING

The work was performed in the framework of the Program of Basic Scientific Research of the Russian Academy of Sciences for 2013–2020, direction III.23.

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Authors and Affiliations

  1. Institute of Strength Physics and Materials Science, Siberian Branch, Russian Academy of Sciences, 634055, Tomsk, Russia

    T. I. Dorofeeva, T. A. Gubaidullina, B. P. Gritsenko & V. P. Sergeev

  2. National Research Tomsk Polytechnic University, 634055, Tomsk, Russia

    B. P. Gritsenko & V. P. Sergeev

Authors
  1. T. I. Dorofeeva
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  2. T. A. Gubaidullina
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  3. B. P. Gritsenko
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  4. V. P. Sergeev
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Correspondence to T. I. Dorofeeva.

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Translated by G. Levit

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Dorofeeva, T.I., Gubaidullina, T.A., Gritsenko, B.P. et al. Structural Phase State and Thermal Cyclic Stability of the Thermal Barrier Zr–Si–O Coatings Deposited on a Copper Substrate by the Microplasma Method. Prot Met Phys Chem Surf 55, 695–699 (2019). https://doi.org/10.1134/S207020511904004X

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