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Synthesis of Graft Copolyimides with Poly(N,N-dimethylamino-2-ethyl methacrylate) Side Chains and Hybrid Nanocomposites with Silver Nanoparticles

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Abstract

The controlled radical polymerization of N,N-dimethylamino-2-ethyl methacrylate on polyimide multicenter macroinitiators under the action of the activating complex of Cu(I) with nitrogen-containing ligands is studied. The complex investigation of the kinetics of copolymerization and the molecular-mass characteristics of the products is performed. The polarity of a medium and the nature of the nitrogen-containing ligand used to prepare the catalytic complex considerably affect the rate of polymerization and the composition and molecular-mass characteristics of the product. Process conditions that enable the synthesis of regularly graft copolyimides with poly(N,N-dimethylamino-2-ethyl methacrylate) side chains are determined. It is shown that the products of grafting copolymerization may be used as a nanoreactor and a stabilizing agent for the template synthesis of composite structures containing silver nanoparticles in the absence of additional reducing agents.

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Authors and Affiliations

  1. Institute of Macromolecular Compounds, Russian Academy of Sciences, St. Petersburg, 199004, Russia

    T. K. Meleshko, A. S. Ivanova, A. V. Kashina, I. V. Ivanov, T. N. Nekrasova, N. V. Zakharova, A. P. Filippov & A. V. Yakimansky

  2. Institute of Chemistry, St. Petersburg State University, Petrodvorets, St. Petersburg, 198504, Russia

    A. V. Yakimansky

Authors
  1. T. K. Meleshko
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  2. A. S. Ivanova
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  3. A. V. Kashina
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  4. I. V. Ivanov
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  5. T. N. Nekrasova
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  6. N. V. Zakharova
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  7. A. P. Filippov
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  8. A. V. Yakimansky
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Corresponding author

Correspondence to A. S. Ivanova.

Additional information

Original Russian Text © T.K. Meleshko, A.S. Ivanova, A.V. Kashina, I.V. Ivanov, T.N. Nekrasova, N.V. Zakharova, A.P. Filippov, A.V. Yakimansky, 2017, published in Vysokomolekulyarnye Soedineniya, Seriya B, 2017, Vol. 59, No. 6, pp. 434–449.

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Meleshko, T.K., Ivanova, A.S., Kashina, A.V. et al. Synthesis of Graft Copolyimides with Poly(N,N-dimethylamino-2-ethyl methacrylate) Side Chains and Hybrid Nanocomposites with Silver Nanoparticles. Polym. Sci. Ser. B 59, 674–688 (2017). https://doi.org/10.1134/S1560090417060045

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