Abstract
Using the liquid-phase methods of synthesis—the coprecipitation of hydroxides and the hydrothermal method—mesoporous xerogels are obtained based on the ZrО2–Y2О3–CeО2 system with 5–8-nm particles and powders (after the heat treatment of xerogels at 600°C) with a coherent scattering region (CSR) size of 9 to 10 nm and Ssp = 96–156 m2/g. After calcination at 1400°C, the powders are transformed into tetragonal solid solutions with a CSR size of 65 nm in the synthesis by the coprecipitation method, and they are transformed into solid solutions with a CSR size of 84 nm with a high degree of tetragonality of c/a = 1.438–1.431 in the synthesis by the hydrothermal method.
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Original Russian Text © N.Yu. Koval’ko, M.V. Kalinina, T.P. Maslennikova, L.V. Morozova, S.V. Myakin, T.V. Khamova, M.Yu. Arsent’ev, O.A. Shilova, 2018, published in Fizika i Khimiya Stekla.
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Koval’ko, N.Y., Kalinina, M.V., Maslennikova, T.P. et al. Comparative Study of Powders Based on the ZrO2–Y2O3–СeO2 System Obtained by Various Liquid Phase Methods of Synthesis. Glass Phys Chem 44, 433–439 (2018). https://doi.org/10.1134/S1087659618050103
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DOI: https://doi.org/10.1134/S1087659618050103