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Fused pyrimidine systems: XIV. Reaction of 2-alkenyl(alkynyl)sulfanylpyrido[3,4-d]pyrimidin-4(3H)-ones with arylsulfanyl chlorides

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Abstract

2-Allylsulfanylpyrido[3,4-d]pyrimidin-4(3H)-one reacted with arylsulfanyl chlorides in chloroform to give addition products to the exocyclic double bond, which were converted into linearly fused arylsulfanylthiazinopyridopyrimidines by the action of sodium acetate. The reactions of 2-allyl(cinnamyl, propargyl)sulfanylpyrido[3,4-d]pyrimidin-4(3H)-ones with arylsulfanyl chlorides in the presence of an equimolar amount of lithium perchlorate afforded angularly fused arylsulfanylmethylthiazolo- and -thiazinopyridopyrimidines.

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Authors and Affiliations

  1. Institute of Organic Chemistry, National Academy of Sciences of Ukraine, ul. Murmanskaya 5, Kiev, 02660, Ukraine

    I. V. Dyachenko, R. I. Vas’kevich & M. V. Vovk

  2. “Kiev Polytechnic Institute” National Technical University of Ukraine, pr. Pobedy 37, Kiev, 03056, Ukraine

    A. I. Vas’kevich

Authors
  1. I. V. Dyachenko
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  2. A. I. Vas’kevich
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  3. R. I. Vas’kevich
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  4. M. V. Vovk
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Corresponding author

Correspondence to A. I. Vas’kevich.

Additional information

Original Russian Text © I.V. Dyachenko, A.I. Vas’kevich, R.I. Vas’kevich, M.V. Vovk, 2014, published in Zhurnal Organicheskoi Khimii, 2014, Vol. 50, No. 6, pp. 874–879.

For communication XIII, see [1].

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Dyachenko, I.V., Vas’kevich, A.I., Vas’kevich, R.I. et al. Fused pyrimidine systems: XIV. Reaction of 2-alkenyl(alkynyl)sulfanylpyrido[3,4-d]pyrimidin-4(3H)-ones with arylsulfanyl chlorides. Russ J Org Chem 50, 858–863 (2014). https://doi.org/10.1134/S1070428014060189

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  • DOI: https://doi.org/10.1134/S1070428014060189

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