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Synthesis of Binuclear Antimony Complexes with Tetraketonate Ligands

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Abstract

Reactions of tetraphenylantimony bromide with sodium salts of 3,8-dioxodeca-4,6-diene-5,6-diol and 2,2,9,9-tetramethyl-3,8-dioxodeca-4,6-diene-5,6-diol at various molar ratios of the reactants have been studied. Irrespective of the molar ratio, binuclear chelate complexes Ph4Sb[OC(R)CHC(O)(O)CCH(R)CO]SbPh4 are formed. The structures of the resulting complexes were established by the methods of IR and NMR spectroscopy.

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Authors and Affiliations

  1. National Research South Ural State University, pr. Lenina 76, Chelyabinsk, 454080, Russia

    E. V. Artem’eva, O. K. Sharutina & V. V. Sharutin

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  1. E. V. Artem’eva
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  2. O. K. Sharutina
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  3. V. V. Sharutin
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Correspondence to E. V. Artem’eva.

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Original Russian Text © E.V. Artem’eva, O.K. Sharutina, V.V. Sharutin, 2017, published in Zhurnal Obshchei Khimii, 2017, Vol. 87, No. 12, pp. 2094–2095.

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Artem’eva, E.V., Sharutina, O.K. & Sharutin, V.V. Synthesis of Binuclear Antimony Complexes with Tetraketonate Ligands. Russ J Gen Chem 87, 2904–2905 (2017). https://doi.org/10.1134/S1070363217120283

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  • DOI: https://doi.org/10.1134/S1070363217120283

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