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Unusual Reaction of 6,8-Dichloro-3,3-dimethyl-7-nitro-3H-2,1,4-benzoxadiazine 4-Oxide with 4-Aminomorpholine

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Abstract

Reaction of 6,8-dichloro-3,3-dimethyl-7-nitro-3H-2,1,4-benzoxadiazine 4-oxide with 4-aminomorpholine occurred through the benzoxadiazine ring opening to form 1,2-bis(2-amino-3,5-dichloro-4-nitrophenyl)-diazene oxide instead of the substitution product.

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References

  1. Miller, M.R. and Megson, I.L., Br. J. Pharmacol., 2007, vol. 151, p. 305. doi 10.1038/sj.bjp.0707224

    Article  CAS  Google Scholar 

  2. Samsonov, V.A., Volodarskii, L.B., and Shamirzaeva, V., Chem. Heterocycl. Compd., 1994, vol. 30, p. 460. doi 10.1007/BF01169943

    Article  Google Scholar 

  3. Chugunova, E., Samsonov, V., Gerasimova, T., Rybalova, T., and Bagryanskaya, I., Tetrahedron, 2015, vol. 71, p. 7233. doi 10.1016/j.tet.2015.03.096

    Article  CAS  Google Scholar 

  4. Chugunova, E.A., Akylbekov, N.I., Gavrilov, N.V., Samsonov, V.A., Sitnov, S.A., Dobrynin, A.B., Pudovik, M.A., and Burilov, A.R., Russ. J. Gen. Chem., 2016, vol. 86, no. 11, p. 2548. doi 10.1134/S1070363216110232

    Article  CAS  Google Scholar 

  5. Chugunova, E.A., Akylbekov, N.I., Samsonov, V.A., Sitnov, S.A., and Burilov, A.R., Russ. J. Org. Chem., 2017, vol. 83, no. 4, p. 637. doi 10.1134/S1070428017040273

    Article  Google Scholar 

  6. Sheldrick, G.M., SADABS. Bruker AXS Inc., Madison, USA, 1997.

    Google Scholar 

  7. Altomare, A., Cascarano, G., Giacovazzo, C., and Viterbo, D., Acta Crystallogr. A, 1991, vol. 47, p. 744. doi 10.1107/S0108767391006566

    Article  Google Scholar 

  8. Sheldrick, G.M., SHELX-97. Program for Crystal Structure Analysis (Release 97-2). University of Göttingen, 1997.

    Google Scholar 

  9. Farrugia, L.J., J. Appl. Crystallogr., 1999, vol. 32, p. 837. doi 10.1107/S0021889899006020

    Article  CAS  Google Scholar 

  10. APEX2 (Version 2.1), SAINTPlus. Data Reduction and Correction Program (Version 7.31A), Bruker Advanced X-ray Solutions, Bruker AXS Inc., Madison, Wisconsin, USA, 2006.

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Authors and Affiliations

  1. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, ul. Akademika Arbuzova 8, Kazan, Tatarstan, 420088, Russia

    E. A. Chugunova & A. R. Burilov

  2. Kazan Federal University, Kazan, Tatarstan, Russia

    E. A. Chugunova

  3. Kazan National Research Technological University, Kazan, Tatarstan, Russia

    N. I. Akylbekov, M. R. Gaziev & A. B. Dobrynin

  4. Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    V. A. Samsonov

Authors
  1. E. A. Chugunova
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  2. N. I. Akylbekov
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  3. M. R. Gaziev
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  4. V. A. Samsonov
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  5. A. B. Dobrynin
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  6. A. R. Burilov
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Corresponding author

Correspondence to E. A. Chugunova.

Additional information

Original Russian Text © E.A. Chugunova, N.I. Akylbekov, M.R. Gaziev, V.A. Samsonov, A.B. Dobrynin, A.R. Burilov, 2017, published in Zhurnal Obshchei Khimii, 2017, Vol. 87, No. 12, pp. 2073–2075.

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Chugunova, E.A., Akylbekov, N.I., Gaziev, M.R. et al. Unusual Reaction of 6,8-Dichloro-3,3-dimethyl-7-nitro-3H-2,1,4-benzoxadiazine 4-Oxide with 4-Aminomorpholine. Russ J Gen Chem 87, 2884–2886 (2017). https://doi.org/10.1134/S1070363217120222

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  • DOI: https://doi.org/10.1134/S1070363217120222

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