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Petroleum Chemistry

, Volume 59, Issue 8, pp 875–879 | Cite as

Synthesis of a Magnetic Core/Shell Nanocomposite Containing Layered Double Hydroxide

  • E. A. Tarasenko
  • I. G. Ryl’tsova
  • M. N. Yapryntsev
  • D. E. Smalchenko
  • O. E. LebedevaEmail author
Article
  • 3 Downloads

Abstract

A method for obtaining a new magnetic nanocomposite Fe3O4@SiO2@Mg/AlFe-LDH with the core/shell structure is described. The procedure for the synthesis of the nanocomposite includes three steps: preparing magnetite nanoparticles, coating the surface of the obtained magnetic nanoparticles with silica, and in situ growing Mg/AlFe-LDH on the Fe3O4@SiO2 surface. Samples obtained at each synthesis step have been characterized using X-ray diffraction analysis and transmission electron microscopy. It has been proved that the layered double hydroxide (LDH) particles “grow” on aggregates of magnetic Fe3O4@SiO2 core/shell nanoparticles and have the so-called “flower-like” morphology.

Notes

FUNDING

The work was supported by the Russian Foundation for Basic Research, project no. 18-29-12103 mk. Used in the study was equipment of the Shared-Use Center “Technologies and Materials” at the Belgorod State University.

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Copyright information

© Pleiades Publishing, Ltd. 2019

Authors and Affiliations

  • E. A. Tarasenko
    • 1
  • I. G. Ryl’tsova
    • 1
  • M. N. Yapryntsev
    • 1
  • D. E. Smalchenko
    • 1
  • O. E. Lebedeva
    • 1
    Email author
  1. 1.Belgorod State National Research UniversityBelgorodRussia

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