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Journal of Structural Chemistry

, Volume 59, Issue 3, pp 635–640 | Cite as

Crystal Structures of New Chalcogenide- Containing Yttrium Orthosilicates Y2SiO4Q (Q = S, Se)

  • A. S. Kiryakov
  • D. A. Piryazev
  • M. S. Tarasenko
  • N. G. Naumov
Article

Abstract

Compounds Y2SiO4Q (Q = S, Se) are obtained by the interaction of oxides and elemental substances in cesium chloride flux. The structures of these compounds are determined by the single crystal XRD analysis. These compounds isostructural and crystallize in the space group Pbcm with the following parameters: Y2SiO4S (I) a = 6.0462(8) Å, b = 6.8976(9) Å, c = 10.6558(13) Å, V = 444.39(10) Å3; Y2SiO4Se (II) a = 5.9935(7) Å, b = 6.9216(8) Å, c = 10.7688(12) Å, V = 446.74(9) Å3. The measured fluxing points are 1650±15 °С for I and 1850±15 °С for II.

Keywords

synthesis yttrium chalcogenide orthosilicate crystal structure 

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Copyright information

© Pleiades Publishing, Ltd. 2018

Authors and Affiliations

  • A. S. Kiryakov
    • 1
    • 2
  • D. A. Piryazev
    • 1
  • M. S. Tarasenko
    • 1
  • N. G. Naumov
    • 1
    • 2
  1. 1.Nikolaev Institute of Inorganic Chemistry, Siberian BranchRussian Academy of SciencesNovosibirskRussia
  2. 2.Novosibirsk State UniversityNovosibirskRussia

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