Abstract
N-Chlorosulfenylsuccinimide is a suitable reagent for the generation of heterocyclic α-oxo thioketones. The latter readily undergo [4 + 2] cycloaddition with 1,3-dienes to give heterocyclic compounds containing spirocyclic thiine substituents.
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Yu. G. Shermolovich and S. V. Emets, Khim. Geterotsikl. Soed., 187 (2000).
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Shermolovich, Y.G., Emets, S.V. & Tolmachev, A.A. Formation of Heterocyclic α-Oxo Thioketones Using N-Chlorosulfenylsuccinimide. Chemistry of Heterocyclic Compounds 39, 1076–1078 (2003). https://doi.org/10.1023/B:COHC.0000003527.43940.ce
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DOI: https://doi.org/10.1023/B:COHC.0000003527.43940.ce