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Synthesis and Crystal Structure of 2,3-Bis(dinitrofluoromethyl)-1,4-dioxane

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

For the first time the dinitromethyl group was modified to dinitrofluoromethyl group in the series of aliphatic polynitro compounds in the case of the reaction of 1,1,4,4-tetranitro-2,3-butanediol diacetate with ammonium fluoroxysulfate in the presence of sodium bicarbonate and ethylene glycol. Previously unknown 2,3-bis(dinitrofluoromethyl)-1,4-dioxane was synthesized. Its structure was determined by X-ray diffraction analysis.

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Authors and Affiliations

  1. Institute of Problems of Chemical Physics, Russian Academy of Sciences, Chernogolovka

    B. S. Fedorov, N. I. Golovina, S. P. Smirnov, I. Sh. Abdrakhmanov, A. I. Firkin & L. O. Atovmyan

  2. State Scientific-Research Institute Kristall, Dzerzhinsk, Russia

    B. S. Fedorov, N. I. Golovina, S. P. Smirnov, I. Sh. Abdrakhmanov, A. I. Firkin & L. O. Atovmyan

Authors
  1. B. S. Fedorov
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  2. N. I. Golovina
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  3. S. P. Smirnov
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  4. I. Sh. Abdrakhmanov
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  5. A. I. Firkin
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  6. L. O. Atovmyan
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Fedorov, B.S., Golovina, N.I., Smirnov, S.P. et al. Synthesis and Crystal Structure of 2,3-Bis(dinitrofluoromethyl)-1,4-dioxane. Chemistry of Heterocyclic Compounds 38, 385–389 (2002). https://doi.org/10.1023/A:1016014802080

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  • DOI: https://doi.org/10.1023/A:1016014802080

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