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Ionic liquid-based microwave-assisted liquid-liquid microextraction and high performance liquid chromatography determination of sulfonamides from animal oils

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Abstract

The authors performed ionic liquid-based microwave-assisted liquid-liquid microextraction(IL-based MALLME) coupled with high performance liquid chromatographic separation for the determination of 6 sulfonamides (SAs) from animal oils. The target analytes were extracted from animal oil samples with sodium hydroxide solution containing 1-butyl-3-methylimidazolium tetrafluoroborateand as the extraction solvent under microwave irradiation. The experimental parameters of the IL-based MALLME, including types of ILs, volume of IL, amount of ion-pairing agent(NH4PF6), pH value of sample solution, and extraction temperature and time were evaluated. The limits of detection and quantification obtained were in a range of 0.4–0.5 μg/kg and a range of 1.2–1.8 μg/kg, respectively. The accuracy of the method was evaluated by analyzing five spiked animal oil samples at two fortified levels(5 and 50 μg/kg), and the recoveries of SAs varied from 81.4% to 114.5% with relative standard deviations ranging from 0.8% to 9.0%.

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Authors and Affiliations

  1. College of Chemistry, Jilin University, Changchun, 130012, P. R. China

    Xu-dong Feng, Rui Su, Li-jie Wu, Xue-yuan Li, Xing-hua Wang, Han-qi Zhang & Ai-min Yu

  2. Department of Pharmacy, Changchun Medical College, Changchun, 130117, P. R. China

    Fang-hui Liang

Authors
  1. Xu-dong Feng
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  2. Fang-hui Liang
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  3. Rui Su
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  4. Li-jie Wu
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  5. Xue-yuan Li
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  6. Xing-hua Wang
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  7. Han-qi Zhang
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  8. Ai-min Yu
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Corresponding author

Correspondence to Ai-min Yu.

Additional information

Supported by the Key Projects of Science and Technology Development Plan of Jilin Province, China(No.20125006) and the Scientific Forefront and Interdisciplinary Innovation Project of Jilin University, China(No.450060481018).

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Feng, Xd., Liang, Fh., Su, R. et al. Ionic liquid-based microwave-assisted liquid-liquid microextraction and high performance liquid chromatography determination of sulfonamides from animal oils. Chem. Res. Chin. Univ. 29, 647–652 (2013). https://doi.org/10.1007/s40242-013-2516-x

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  • DOI: https://doi.org/10.1007/s40242-013-2516-x

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