Abstract
The microwave-absorption capabilities of high-alumina fly ash (HAFA), Na2CO3 and HAFA–Na2CO2 mixtures were investigated by determining the dielectric properties [real part (ε′), imaginary part (ε″) and dielectric loss tangent (tan δ)] from 25°C to 800°C, using the microwave resonant cavity technique at a microwave frequency of 2450 MHz. The mass ratio of the HAFA–Na2CO3 mixtures used in all experiments was 1:1. The study found that the microwave absorption capabilities of HAFA alone do not change significantly within the range of temperatures examined. For both Na2CO3 and HAFA–Na2CO3 mixtures, however, a sharp increase in absorption capability was observed above 400°C. The microwave heating behavior of the HAFA–Na2CO3 mixtures can be divided into two stages: in the first stage (< 350°C), heating rates were found to be lower due to the weaker microwave absorption capability of the HAFA and Na2CO3; however, in the second stage (≥ 350°C), a sharp increase in heating rate was observed, linked to the strengthened absorption capability of the Na2CO3. The study found that HAFA–Na2CO3 mixtures have a good microwave-absorption ability and can be heated rapidly by microwaves; therefore, it is feasible to use microwave heating for the activation of high-alumina fly ash with Na2CO3.
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Acknowledgements
The authors are grateful for the financial support by the National Key R& D Program of China (No. 2017YFB0603101) and the National Natural Science Foundation of China (51764034).
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Zhou, B., Zhou, J., Zhang, L. et al. Heating Mechanism of High Aluminum Fly Ash Activated by Na2CO3 in Microwave Field. JOM 71, 2959–2965 (2019). https://doi.org/10.1007/s11837-019-03535-3
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DOI: https://doi.org/10.1007/s11837-019-03535-3