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Enhanced Mechanical Properties of ECAPed Mg-9Al-1Si Alloy by a Two-Stage Pretreatment

  • Second-Phase Particles in Magnesium Alloys: Engineering for Properties and Performance
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Abstract

A two-stage pretreatment (TSP), namely ultrasonic vibration treatment and solid-solution treatment, is proposed to improve the microstructure and properties of Mg-9Al-1Si alloy before equal-channel angular pressing (ECAP). The ultrasonic vibration treatment could distribute Mg2Si and Mg17Al12 phases uniformly in the alloy, while alloys subjected to solid-solution treatment exhibited a reduction in the amount of Mg17Al12 phase and improved plastic deformation capacity. In addition, the microstructure can be significantly refined, and broken Mg2Si phase and fine Mg17Al12 precipitates can reduce the average grain size during the ECAP process. Therefore, the strength and elongation of the ECAPed Mg-9Al-1Si alloy were improved simultaneously by introducing the TSP. The yield strength, ultimate tensile strength, and elongation of the ECAPed alloy with TSP were significantly enhanced to 290 MPa, 350 MPa, and 14.77%, respectively.

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References

  1. N.V. Ravi Kumar, J.J. Blandin, C. Desrayaud, F. Montheillet, and M. Suéry, Mater. Sci. Eng. A 359, 150 (2003).

    Article  Google Scholar 

  2. R.M. Wang, A. Eliezer, and E. Gutman, Mater. Sci. Eng. A 344, 279 (2003).

    Article  Google Scholar 

  3. J. Yang, D.R. Ni, D. Wang, B.L. Xiao, and Z.Y. Ma, Mater. Charact. 96, 142 (2014).

    Article  Google Scholar 

  4. A. Srinivasan, J. Swaminathan, U.T.S. Pillai, K. Guguloth, and B.C. Pai, Mater. Sci. Eng. A 485, 86 (2008).

    Article  Google Scholar 

  5. Z.W. Wang, H.X. Wang, J.L. Gong, M. Li, W.L. Cheng, and W. Liang, China Foundry 13, 310 (2016).

    Article  Google Scholar 

  6. G.Y. Yuan, Z.L. Liu, Q.D. Wang, and W.J. Ding, Mater. Lett. 56, 53 (2002).

    Article  Google Scholar 

  7. J. Gong, W. Liang, H. Wang, X. Zhao, and L. Bian, Rare. Met. Mater. Eng. 42, 1800 (2013).

    Article  Google Scholar 

  8. F. Xue, X. Min, and Y. Sun, J. Mater. Sci. 41, 4725 (2006).

    Article  Google Scholar 

  9. E. Mostaed, A. Fabrizi, D. Dellasega, F. Bonollo, and M. Vedani, J. Alloys Compd. 638, 267 (2015).

    Article  Google Scholar 

  10. H.K. Lin, J.C. Huang, and T.G. Langdon, Mater. Sci. Eng. A 402, 250 (2005).

    Article  Google Scholar 

  11. W.L. Cheng, L. Tian, H.X. Wang, L.P. Bian, and H. Yu, Mater. Sci. Eng. A 687, 148 (2017).

    Article  Google Scholar 

  12. W. Wang, H. Wang, Y. Liu, H. Nie, and W. Cheng, J. Mater. Res. 32, 615 (2017).

    Article  Google Scholar 

  13. M. Shahzad, A.H. Qureshi, and H. Waqas, Mater. Des. 51, 870 (2013).

    Article  Google Scholar 

  14. P. Palai, N. Prabhu, P.D. Hodgson, and B.P. Kashyap, J. Mater. Eng. Perform. 23, 77 (2014).

    Article  Google Scholar 

  15. L. Zhang, Q. Wang, W. Liao, W. Guo, B. Ye, H. Jiang, and W. Ding, J. Mater. Sci. Technol. 33, 935 (2017).

    Article  Google Scholar 

  16. Y.Z. Uuml, Q.D. Wang, X.Q. Zeng, Y.P. Zhu, and W.J. Ding, Mater. Sci. Eng. A 301, 255 (2001).

    Article  Google Scholar 

  17. X. Liu, Y. Osawa, S. Takamori, and T. Mukai, Mater. Sci. Eng. A 487, 120 (2008).

    Article  Google Scholar 

  18. X. Jian, T.T. Meek, and Q. Han, Scr. Mater. 54, 893 (2006).

    Article  Google Scholar 

  19. K.B. Nie, X.J. Wang, K. Wu, M.Y. Zheng, and X.S. Hu, Mater. Sci. Eng. A 528, 7484 (2011).

    Article  Google Scholar 

  20. K.B. Nie, X.J. Wang, K. Wu, X.S. Hu, M.Y. Zheng, and L. Xu, Mater. Sci. Eng. A 528, 8709 (2011).

    Article  Google Scholar 

  21. J.T. Zhang, Y.G. Zhao, X.U. Xiao-Feng, and X.B. Liu, Trans. Nonferrous Met. Soc. 23, 2852 (2013).

    Article  Google Scholar 

  22. H. Yan, Y. Rao, and R. He, J. Mater. Process. Technol. 214, 612 (2014).

    Article  Google Scholar 

  23. M. Ben-Haroush, G. Ben-Hamu, D. Eliezer, and L. Wagner, Corros. Sci. 50, 1766 (2008).

    Article  Google Scholar 

  24. L. Zheng, H. Nie, W. Zhang, W. Liang, and Y. Wang, Mater. Sci. Eng. A 722, 58 (2017).

    Article  Google Scholar 

  25. S.H. Park, S.H. Kim, Y.M. Kim, and B.S. You, J. Alloys Compd. 646, 932 (2015).

    Article  Google Scholar 

  26. L. Zheng, H. Nie, W. Liang, H. Wang, and Y. Wang, J. Magnes. Alloys 4, 115 (2016).

    Article  Google Scholar 

  27. H. Wang, B. Zhou, Y. Zhao, K. Zhou, W. Cheng, and W. Liang, Mater. Sci. Eng. A 589, 119 (2014).

    Article  Google Scholar 

  28. W. Wang, H. Wang, G. Ren, W. Cheng, and S. Zhang, Rare. Met. Mater. Eng. 46, 2847 (2017).

    Article  Google Scholar 

  29. W. Tang, S. Huang, S. Zhang, D. Li, and Y. Peng, J. Mater. Process. Technol. 211, 1203 (2011).

    Article  Google Scholar 

  30. H. Lim, M.G. Lee, J.H. Kim, B.L. Adams, and R.H. Wagoner, Int. J. Plast. 27, 1328 (2011).

    Article  Google Scholar 

  31. T. Al-Samman, Mater. Sci. Eng. A 560, 561 (2013).

    Article  Google Scholar 

  32. W.L. Cheng, Q.W. Tian, H. Yu, H. Zhang, and B.S. You, J. Magnes. Alloys 2, 299 (2014).

    Article  Google Scholar 

  33. W.J. Li, K.K. Deng, X. Zhang, K.B. Nie, and F.J. Xu, Mater. Sci. Eng. A 677, 367 (2016).

    Article  Google Scholar 

  34. K.B. Nie, K.K. Deng, X.J. Wang, T. Wang, and K. Wu, Mater. Charact. 124, 14 (2017).

    Article  Google Scholar 

  35. S. Khani, M.R. Aboutalebi, M.T. Salehi, H.R. Samim, and H. Palkowski, Mater. Sci. Eng. A 678, 44 (2016).

    Article  Google Scholar 

  36. C. Bettles and M. Gibson, JOM 57, 46 (2005).

    Article  Google Scholar 

  37. F.A. Mirza, D.L. Chen, D.J. Li, and X.Q. Zeng, Mater. Des. 46, 411 (2013).

    Article  Google Scholar 

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Acknowledgements

The authors gratefully acknowledge financial support from the Natural Science Foundation of Shanxi Province (201701D121045), National Natural Science Foundation of China (51301118, 51404166), and Shanxi Province Scientific Facilities and Instruments Shared Service Platform (201805D141005).

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Correspondence to Hongxia Wang or Weili Cheng.

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Zhang, Z., Wang, H., Wang, Z. et al. Enhanced Mechanical Properties of ECAPed Mg-9Al-1Si Alloy by a Two-Stage Pretreatment. JOM 71, 2178–2186 (2019). https://doi.org/10.1007/s11837-019-03439-2

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  • DOI: https://doi.org/10.1007/s11837-019-03439-2

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