Abstract
In-situ TEM nanoindentation of a polycrystalline Cu film was cross-correlated with precession electron diffraction (PED) to quantify the microstructural evolution. The use of PED is shown to clearly reveal features, such as grain size, that are easily masked by diffraction contrast created by the deformation. Using PED, the accompanying grain refinement and change in texture as well as the preservation of specific grain boundary structures, including a ∑3 boundary, under the indent impression were quantified. The nucleation of dislocations, evident in low-angle grain boundary formations, was also observed under the indent. PED quantification of texture gradients created by the indentation process linked well to bend contours observed in the bright-field images. Finally, PED enabled generating a local orientation spread map that gave an approximate estimation of the spatial distribution of strain created by the indentation impression.
Similar content being viewed by others
References
M. Jin, A.M. Minor, E.A. Stach, and J.W. Morris, Acta Mater. 52, 5381 (2004).
L. Wang, J. Teng, P. Liu, A. Hirata, E. Ma, Z. Zhang, M. Chen, and X. Han, Nature Commun. 5, 4402 (2014).
T. Rupert, D. Gianola, Y. Gan, and K. Hemker, Science 326, 1686 (2009).
M. Ojima, Y. Adachi, S. Suzuki, and Y. Tomota, Acta Mater. 59, 4177 (2011).
T. Ruggles, D. Fullwood, and J. Kysar, Int. J. Plast 76, 231 (2016).
P.J. Hurley and F.J. Humphreys, Acta Mater. 51, 1087 (2003).
M. Calcagnotto, D. Ponge, E. Demir, and D. Raabe, Mater. Sci. Eng. A 527, 2738 (2010).
M. Legros, D.S. Gianola, and K.J. Hemker, Acta Mater. 56, 3380 (2008).
S.P. Deshmukh, R.S. Mishra, and I.M. Robertson, Mater. Sci. Eng. A 527, 2390 (2010).
N. Li, J. Wang, A. Misra, and J.Y. Huang, Microsc. Microanal. 18, 1155 (2012).
E. Hintsala, D. Kiener, J. Jackson, and W.W. Gerberich, Exp. Mech. 55, 1681 (2015).
Q. Yu, J. Sun, J.W. Morris, and A.M. Minor, Scr. Mater. 69, 57 (2013).
A. Avilov, K. Kuligin, S. Nicolopoulos, M. Nickolskiy, K. Boulahya, J. Portillo, G. Lepeshov, B. Sobolev, J.P. Collette, N. Martin, A.C. Robins, and P. Fischione, Ultramicroscopy 107, 431 (2007).
P. Moeck, S. Rouvimov, E. Rauch, M. Véron, H. Kirmse, I. Häusler, W. Neumann, D. Bultreys, Y. Maniette, and S. Nicolopoulos, Cryst. Res. Technol. 46, 589 (2011).
E. Rauch and M. Véron, Mater. Charact. 98, 1 (2014).
J. Roqué Rosell, J. Portillo Serra, T. Aiglsperger, S. Plana-Ruiz, T. Trifonov, and J.A. Proenza, J. Cryst. Growth 483, 228 (2018).
P.K. Suri, J.E. Nathaniel, C.M. Barr, J.K. Baldwin, K. Hattar, and M.L. Taheri, Microsc. Microanal. 23, 2236 (2017).
I. Ghamarian, Y. Liu, P. Samimi, and P.C. Collins, Acta Mater. 79, 203 (2014).
D.C. Bufford, D. Stauffer, W.M. Mook, S. Syed Asif, B.L. Boyce, and K. Hattar, Nano Lett. 16, 4946 (2016).
A. Kobler, A. Kashiwar, H. Hahn, and C. Kübel, Ultramicroscopy 128, 68 (2013).
A. Gouldstone, N. Chollacoop, M. Dao, J. Li, A.M. Minor, and Y.-L. Shen, Acta Mater. 55, 4015 (2007).
L.A. Giannuzzi and F.A. Stevie, Micron 30, 197 (1999).
K. Thompson, D. Lawrence, D.J. Larson, J.D. Olson, T.F. Kelly, and B. Gorman, Ultramicroscopy 107, 131 (2007).
G.B. Thompson, M.K. Miller, and H.L. Fraser, Ultramicroscopy 100, 25 (2004).
P.J. Felfer, T. Alam, S.P. Ringer, and J.M. Cairney, Microsc. Res. Tech. 75, 484 (2012).
J. Ciston, B. Deng, L.D. Marks, C.S. Own, and W. Sinkler, Ultramicroscopy 108, 514 (2008).
D.B. Williams and C.B. Carter, Transmission Electron Microscopy, 2nd ed. (New York: Springer, 2009), pp. 389–416.
Z. Basinski, A. Korbel, and S. Basinski, Acta Metall. 28, 191 (1980).
Q. Guo, Y.S. Chun, J.H. Lee, Y.-U. Heo, and C.S. Lee, Met. Mater. Int. 20, 1043 (2014).
L. Lu, Y. Shen, X. Chen, L. Qian, and K. Lu, Science 304, 422 (2004).
K. Lu, L. Lu, and S. Suresh, Science 324, 349 (2009).
C.A. Schuh, M. Kumar, and W.E. King, J. Mater. Sci. 40, 847 (2005).
A.C. Leff, C.R. Weinberger, and M.L. Taheri, Ultramicroscopy 153, 9 (2015).
D. Cooper, T. Denneulin, N. Bernier, A. Béché, and J.-L. Rouvière, Micron 80, 145 (2016).
A. Minor, E. Lilleodden, E. Stach, and J. Morris, J. Mater. Res. 19, 176 (2004).
F. Dalla Torre, H. Van Swygenhoven, and M. Victoria, Acta Mater. 50, 3957 (2002).
D.A. Porter, K.E. Easterling, and M.Y. Sherif, Phase Transformations in Metals and Alloys, 3rd ed. (Boca Raton: CRC Press, 2009), pp. 111–179.
Y. Zhang, G.J. Tucker, and J.R. Trelewicz, Acta Mater. 131, 39 (2017).
R.Z. Valiev and T.G. Langdon, Prog. Mater Sci. 51, 881 (2006).
C. Reuber, P. Eisenlohr, F. Roters, and D. Raabe, Acta Mater. 71, 333 (2014).
Z. Hu, M. Farahikia, and F. Delfanian, J. Compos. Mater. 49, 3359 (2015).
Acknowledgements
The authors gratefully acknowledge ARO W911NF-17-1-0528, Dr. Michael Bakas Program Manager. The Bruker PI-95 indenter was acquired through the NSF-DMR-1531722.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Guo, Q., Thompson, G.B. In-situ Indentation and Correlated Precession Electron Diffraction Analysis of a Polycrystalline Cu Thin Film. JOM 70, 1081–1087 (2018). https://doi.org/10.1007/s11837-018-2854-8
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11837-018-2854-8