Skip to main content

Advertisement

Log in

Effect of Tempering Temperature on the Microstructure and Properties of Fe-2Cr-Mo-0.12C Pressure Vessel Steel

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

To obtain the high-temperature strength and toughness of the medium–high-temperature–pressure steel, the microstructure evolution and mechanical properties of Fe-2Cr-Mo-0.12C steel subjected to three different tempering temperatures after being normalized were investigated. The results show that the microstructure of the sample, tempered in the range 675-725 °C for 50 min, did not change dramatically, yet the martensite/austenite constituents decomposed, and the bainite lath merged together and transformed into polygonal ferrite. At the same time, the precipitate size increased with an increase in tempering temperature. With the increase in the tempering temperature from 675 to 725 °C, the impact absorbed energy of the Fe-2Cr-Mo-0.12C steel at −40 °C increased from 257 to 325 J, and the high-temperature yield strength decreased; however, the high-temperature ultimate tensile strength tempered at 700 °C was outstanding (422-571 MPa) at different tested temperatures. The variations of the properties were attributed to the decomposition of M/A constituents and the coarsening of the precipitates. Fe-2Cr-Mo-0.12C steel normalized at 930 °C and tempered at 700 °C was found to have the best combination of ductility and strength.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8

Similar content being viewed by others

References

  1. J.Z. Tan and Y.J. Chao, Effect of Service Exposure on the Mechanical Properties of 2.25Cr-1Mo Pressure Vessel Steel in a Hot-Wall Hydrofining Reactor, Mater. Sci. Eng. A, 2005, 405, p 214–220

    Article  Google Scholar 

  2. H.K.D.H. Bhadeshia, Bainite in Steels, The Institute of Materials, London, 1992, p 329–346

    Google Scholar 

  3. R. Davis et al., Metals Handbook, Vol 1, 10th ed., ASM International, USA, 1990, p 617–652

    Google Scholar 

  4. N.S. Cheruvu, Degradation of Mechanical Properties of Cr-Mo-V and 2.25Cr-1Mo Steel Components After Long-Term Service at Elevated Temperatures, Metall. Trans. A, 1989, 20(1), p 87–95

    Article  Google Scholar 

  5. R.C. Thomson and H.K.D.H. Bhadeshia, Changes in Chemical Composition of Carbides in 2.25Cr-1Mo Power Plant Steel: Part I, Bainitic Microstructure, Mater. Sci. Technol., 1994, 10(3), p 193–204

    Article  Google Scholar 

  6. R.G. Baker and J. Nutting, Tempering of 2.25Cr-1Mo Steel After Quenching and Normalization, J. Iron Steel Inst., 1959, 192(7), p 257–263

    Google Scholar 

  7. M.C. Tsai, C.S. Chiou, and J.R. Yang, Microstructural Evolution of Simulated Heat-Affected Zone in Modified 2.25Cr-1Mo Steel During High Temperature Exposure, Mater. Sci. Eng. A, 2003, 38(11), p 2373–2391

    Google Scholar 

  8. J. Janovec, M. Svoboda, and A. Kroupa, Thermal-Induced Evolution of Secondary Phases in Cr-Mo-V Low Alloy Steels, Mater. Sci. Eng. A, 2006, 41(1), p 3425–3433

    Google Scholar 

  9. M.A. Islam, P. Bowen, and J.F. Knott, Intergranular Fracture on Fatigue Fracture Surface of 2.25Cr-1Mo Steel at Room Temperature in Air, J. Mater. Eng. Perform., 2005, 14, p 28–36

    Article  Google Scholar 

  10. K. Miyata and Y. Sawaragi, Effect of Mo and W on the Phase Stability of Precipitates in Low Cr Heat Resistant Steels, ISIJ Int., 2001, 41, p 281–289

    Article  Google Scholar 

  11. J. Chen, F.S. Pan, and R.L. Zuo, Effect of Mo on Microstructure and Property of Fire-Resistant Steel, Iron Steel Vanadium Titan., 2007, 28, p 24–27

    Google Scholar 

  12. S. Sankaran, V.S. Sarma, and K.A. Padmanabhan, High Cycle Fatigue Behaviour of a Multiphase Microalloyed Medium Carbon Steel: A Comparison Between Ferrite–Pearlite and Tempered Martensite Microstructures, Mater. Sci. Eng. A, 2003, 362, p 249–256

    Article  Google Scholar 

  13. S. Sankaran, V.S. Sarma, and K.A. Padmanabhan, Low Cycle Fatigue Behavior of a Multiphase Microalloyed Medium Carbon Steel: Comparison Between Ferrite–Pearlite and Quenched and Tempered Microstructures, Mater. Eng. A-struct. Mater. Prop. Microstruct. Process., 2003, 345, p 328–335

    Article  Google Scholar 

  14. ISO6892-1, Metallic Materials–Tensile Testing—Part 1: Method of Test at Room Temperature, 2009 (in Chinese).

  15. Y. Zhou, T. Jia, X. Zhang, Z. Liu, and R.D.K. Misra, Investigation on Tempering of Granular Bainite in an Offshore Platform Steel, Mater. Sci. Eng. A, 2015, 626, p 352–361

    Article  Google Scholar 

  16. G. Krauss, Steels Processing Structure and performance (Springer, 2005), pp. 123−125, 252−256.

  17. S.W. Yang, C.J. Shang, X.L. He, X.M. Wang, and Y. Yuan, Stability of Ultra-Fine Microstructure During Tempering, J. Univ. Sci. Technol. Beijing, 2001, 8(3), p 119–122

    Google Scholar 

  18. P. Parameswaran, M. Vijayalakshmi, and V.S. Raghunathan, The Influence of Prior Microstructure on Tempering Stages in 2.25Cr-lMo Steel, High Temp. Mater. Process. (London), 2002, 21, p 251–267

    Article  Google Scholar 

  19. L. Ceschini, A. Marconi, C. Martini, A. Morri, and A. Di Schino, Tensile and Impact Behaviour of a Microalloyed Medium Carbon Steel: Effect of the Cooling Condition and Corresponding Microstructure, Mater. Des., 2013, 45, p 171–178

    Article  Google Scholar 

  20. P. Zhao and D.J. Boyd, Microstructure–property Relationships in Thermomechanically Processed Micro Alloyed Medium Carbon Steels, Mater. Sci. Technol., 2004, 20, p 695–704

    Article  Google Scholar 

  21. Zhang Jie, Cai Qing-wu, and Wu Hui-bin, Effect of Tempering Temperature on Microstructure and Properties of E690 Offshore Plate Steel, J. Iron. Steel Res. Int., 2012, 19, p 67–72

    Google Scholar 

  22. A. Chatterjee, D. Chakrabarti, A. Moitra, R. Mitra, and A.K. Bhaduri, Effect of Normalization Temperatures on Ductile–Brittle Transition Temperature of a Modified 9Cr-1Mo Steel, Mater. Sci. Eng., A, 2014, 618, p 219–231

    Article  Google Scholar 

  23. P.J. Ennis and A. Czyrska-Filemonowicz, Recent Advances in Creep-Resistant Steels for Power Plant Applications, Sadhana, 2003, 28(3–4), p 709–730

    Article  Google Scholar 

  24. X.Z. Zhang and J.F. Knott, Cleavage Fracture in Bainitic and Martensitic Microstructures, Acta Mater., 1999, 47(12), p 3483–3495

    Article  Google Scholar 

  25. Changsheng Li, Biao Ma, Tao Li, and Tao Zhu, Microstructure and Mechanical Properties of 1000 MPa Ultra-High Strength Hot Rolled Plate Steel for Coal Mine Refuge Chamber, Acta Metall. Sin. (English Letters), 2014, 27(3), p 422–429

    Article  Google Scholar 

Download references

Acknowledgments

The authors are very grateful to the financial support of the National Natural Science Foundation of China (51274062) and Research Fund for the Doctoral Program of Higher Education of China (20130042110040).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Chang-sheng Li.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Wang, Qw., Li, Cs., Peng, H. et al. Effect of Tempering Temperature on the Microstructure and Properties of Fe-2Cr-Mo-0.12C Pressure Vessel Steel. J. of Materi Eng and Perform 27, 1485–1493 (2018). https://doi.org/10.1007/s11665-017-2856-7

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-017-2856-7

Keywords

Navigation