Advertisement

Russian Chemical Bulletin

, Volume 53, Issue 8, pp 1722–1725 | Cite as

Synthesis of substituted 1-thia-3-aza-λ5-phosphacyclohex-2-ene

  • M. A. Pudovik
  • S. A. Terent’va
  • N. A. Khailova
  • R. Z. Musin
  • N. M. Azancheev
  • O. N. Kataeva
  • I. A. Litvinov
  • A. B. Dobrynin
  • A. N. Pudovik
Article

Abstract

The addition of dimethylamine to O-phenyl 2-chloropropylisothiocyanatophosphonate afforded the six-membered cyclic product, viz., 1-thia-3-aza-4λ5-phosphacyclohex-2-ene.

Key words

chloroalkylphosphonates functionalization heterocyclization thiaazaphosphacyclohexene 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    Khailova, N. A., Krepysheva, N. E., Saakyan, G. M., Bagautdinova, R. Kh., Shaimardanova, A. A., Zyablikova, T. A., Azancheev, N. M., Litvinov, I. A., Gubaidullin, A. T., Zverev, V. V., Pudovik, M. A., Pudovik, A. N. 2002Zh. Obshch. Khim.721145[Russ. J. Gen. Chem., 2002, 72 (Engl. Transl.)]Google Scholar
  2. 2.
    Kabachnik, M. I., Rossiiskaya, P. A. 1946Izv. AN. Otd. Khim. Nauk3295[Bull. Acad. Sci., Div. Chem. Sci.] (in Russian)Google Scholar
  3. 3.
    Chmutova, G. A., Zverev, V. V., Pudovik, M. A., Khailova, N. A., Pudovik, A. N. 2003Zh. Obshch. Khim.731793[Russ. J. Gen. Chem., 2003, 73 (Engl. Transl.)]Google Scholar
  4. 4.
    Spek, A. L. 1998PLATON for Windows, Version 98, Acta Crystallogr., Sect. A4634Google Scholar
  5. 5.
    Walsh, E. N. 1959J. Am. Chem. Soc.313023Google Scholar
  6. 6.
    Altomare, A., Cascarano, G., Giacovazzo, C., Viterbo, D. 1991Acta Crystallogr., Sect. A47744Google Scholar
  7. 7.
    L. H. Straver and A. J. Schierbeek, MOLEN. Structure Determination System, Vol. 1. Program Description, Nonius B. V., 1994, 180.Google Scholar
  8. 8.
    Hamilton, W. C. 1965Acta Crystallogr.18502Google Scholar

Copyright information

© Springer Science+Business Media, Inc. 2004

Authors and Affiliations

  • M. A. Pudovik
    • 1
  • S. A. Terent’va
    • 1
  • N. A. Khailova
    • 1
  • R. Z. Musin
    • 1
  • N. M. Azancheev
    • 1
  • O. N. Kataeva
    • 1
  • I. A. Litvinov
    • 1
  • A. B. Dobrynin
    • 1
  • A. N. Pudovik
    • 1
  1. 1.A. E. Arbuzov Institute of Organic and Physical ChemistryKazan Research Center of the Russian Academy of SciencesKazanRussian Federation

Personalised recommendations