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Research on Chemical Intermediates

, Volume 41, Issue 11, pp 8829–8838 | Cite as

Effect of ultrasonic radiation’s times to the control size of silver nanoparticles in κ-carrageenan

  • Randa Fawzi Elsupikhe
  • Kamyar Shameli
  • Mansor B. Ahmad
Article

Abstract

The sonochemical method as a green method for the preparation and size control of silver nanoparticles (Ag-NPs) formed in κ-carrageenan has been developed. κ-carrageenan was chosen because it is an eco-friendly stabilizer and ultrasonic irradiation reducing agent. Formations of Ag/κ-carrageenan were determined by electronic spectroscopy where the surface plasmon absorption maxima were observed at 437–412 nm. The FT-IR spectrum indicated the presence of κ-carrageenan in capping with Ag-NPs. The XRD analysis proved that the Ag-NPs were of a face-centered cubic structure. TEM images displayed well-dispersed Ag-NPs with an average particle size of less than 10 nm. SEM images indicated the spherical shape of the Ag-NPs.

Keywords

Green method Ultrasonic irradiation Silver nanoparticles κ-Carrageenan Silver nitrate 

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Copyright information

© Springer Science+Business Media Dordrecht 2015

Authors and Affiliations

  1. 1.Department of Chemistry, Faculty of ScienceUniversiti Putra MalaysiaSerdangMalaysia
  2. 2.Malaysia-Japan International Institute of Technology (MJIIT)Universiti Teknologi MalaysiaKuala LumpurMalaysia

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