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Effect of ultrasonic radiation’s times to the control size of silver nanoparticles in κ-carrageenan

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Abstract

The sonochemical method as a green method for the preparation and size control of silver nanoparticles (Ag-NPs) formed in κ-carrageenan has been developed. κ-carrageenan was chosen because it is an eco-friendly stabilizer and ultrasonic irradiation reducing agent. Formations of Ag/κ-carrageenan were determined by electronic spectroscopy where the surface plasmon absorption maxima were observed at 437–412 nm. The FT-IR spectrum indicated the presence of κ-carrageenan in capping with Ag-NPs. The XRD analysis proved that the Ag-NPs were of a face-centered cubic structure. TEM images displayed well-dispersed Ag-NPs with an average particle size of less than 10 nm. SEM images indicated the spherical shape of the Ag-NPs.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400, Serdang, Selangor, Malaysia

    Randa Fawzi Elsupikhe & Mansor B. Ahmad

  2. Malaysia-Japan International Institute of Technology (MJIIT), Universiti Teknologi Malaysia, Jalan Sultan Yahya Petra (Jalan Semarak), 54100, Kuala Lumpur, Malaysia

    Kamyar Shameli

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  1. Randa Fawzi Elsupikhe
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  2. Kamyar Shameli
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  3. Mansor B. Ahmad
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Correspondence to Kamyar Shameli or Mansor B. Ahmad.

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Elsupikhe, R.F., Shameli, K. & Ahmad, M.B. Effect of ultrasonic radiation’s times to the control size of silver nanoparticles in κ-carrageenan. Res Chem Intermed 41, 8829–8838 (2015). https://doi.org/10.1007/s11164-015-1931-7

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  • DOI: https://doi.org/10.1007/s11164-015-1931-7

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