Skip to main content
Log in

Agglomerates in nanopowders and ceramic technology

  • Scientific Research and Development
  • Published:
Refractories and Industrial Ceramics Aims and scope

Questions are considered connected with use in ceramic technology of ultrafine powder raw material with agglomerated particles. It is shown that presence of agglomerates in nanopowders unavoidably leads to formation in sintered material of structural defects in the form of residual porosity and microcracks. Data are provided for a quantitative dependence of pore structure characteristics for a powder compact on the content of agglomerated particles and the connection of pore structure characteristics with sintering kinetics and the properties of the sintered material obtained.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

References

  1. F. F. Lange, “Powder processing science and technology for increased reliability,” J. Amer. Ceram. Soc., 72, No. 1, 3 – 15 91989).

    Article  CAS  Google Scholar 

  2. F. F. Lange, “Sinterability of agglomerated powders,” J. Amer. Ceram. Soc., 67, No. 2, 83 – 88 (1984).

    Article  CAS  Google Scholar 

  3. W. H. Rhodes, “Agglomerate particle size effects on sintering yttria-stabilized zirconia,” J. Amer. Ceram. Soc., 64, No. 1, 19 – 22 (1981).

    Article  CAS  Google Scholar 

  4. M. A. C. G. Van de Graaf, J. H. H. Ter Maat, and A. J. Burggraaf, “Microstructure and sintering kinetics of highly reaction ZrO2–Y2O3 ceramics,” J. Mater. Sci., 20, 1407 – 1418 (1988).

    Article  ADS  Google Scholar 

  5. A. V. Galakhov, V. Ya. Shevchenko, and V. Ya. Shevchenko, “Influence of pore structure inhomogeneities in green compacts on strength and reliability of Y-TZP,” J. Europ. Ceram. Soc., 6, 317 – 322 (1990).

    Article  Google Scholar 

  6. F. F. Lange and M. Metcalf, “ Processing-related fracture origins: II. Agglomerate motion and crack-like internal surfaces caused by differential sintering,” J. Amer. Ceram. Soc., 67, No. 9, 596 – 601 (1984).

    Article  Google Scholar 

  7. A. V. Galakhov, V. A. Kryuchkov, A. V. Prokov’ev, et al., “Effect of forming pressure on sintering capacity of submicron powders of tetragonal zirconium oxide,” Ogneupory, No. 2, 5 – 11 91993).

  8. A. V. Galakhov, I. V. Vyazov, V. Ya. Shevchenko, et al., “Effect of pore structure of molding submicron powders on the strength of zirconium dioxide ceramic,” Izv. Akad. Nauk SSSR, Neorgan. Materially, 26, No. 4, 828 – 833 (1990).

    Google Scholar 

  9. G. L. Messing, S. C. Zhang, and G. V. Jayanthi, “Ceramic powder synthesis by spray pyrolysis,” J. Amer. Ceram. Soc., 76, No. 11, 2707 – 2726 (1993).

    Article  CAS  Google Scholar 

  10. G. Lipson and G. Steel, Interpretation of Powder x-ray Patterns [Russian translation], Mir, Moscow (1972).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Additional information

Translated from Novye Ogneupory, No. 9, pp. 20 – 25, September 2009.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Galakhov, A.V. Agglomerates in nanopowders and ceramic technology. Refract Ind Ceram 50, 348–353 (2009). https://doi.org/10.1007/s11148-010-9212-x

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11148-010-9212-x

Keywords

Navigation