Advertisement

Measurement Techniques

, Volume 58, Issue 3, pp 362–366 | Cite as

The Use of Optical Methods of Measurement to Investigate the Composition of New Aviation Materials

  • T. N. Zagvozdkina
  • F. N. Karachevtsev
  • R. M. Dvoretskov
  • E. A. Mekhanik
Article
  • 26 Downloads

A procedure for the microwave sample preparation of nickel alloys to determine the mass fractions of Al, Ti, Cr, Co, Nb, Mo, Ru, Ta, W, and Re by atomic-emission spectrometry with an inductively coupled plasma is described. The compositions of the mixtures for solution and the parameters of the microwave dispersion are chosen. The limits of the relative error in measuring the mass fraction of the elements from 0.1% to 20% do not exceed 4% (P = 0.95).

Keywords

microwave sample preparation nickel alloys atomic-emission spectrometry with inductively coupled plasma 

References

  1. 1.
    A. A. Papyshev and D. A. Danilova, “The use of atomic-emission spectrometry with an inductively coupled plasma to analyze materials and products of ferrous metallurgy,” Analit. Kontrol, 11, No. 2–3, 131–181 (2007).Google Scholar
  2. 2.
    E. A. Tormysheva, E. V. Smirnova, and T. N. Ermolaeva, “Microwave sample preparation of fused materials for analysis by atomic-emission spectroscopy with an inductively coupled plasma,” Zavod. Lab. Diagn. Mater., 76, No. 10, 10–13 (2010).Google Scholar
  3. 3.
    E. N. Kablov, G. A. Morozov, V. N. Krutikov, and N. P. Muravskaya, “Certification of standard samples of a compound of multiply-doped alloys using a standard,” Aviats. Mater. Tekhnol., No. 2, 9–11 (2012).Google Scholar
  4. 4.
    A. F. Letov, F. N. Karachevtsev, N. V. Gundobin and V. I. Titov, “The development of standard samples of a compound of alloys for aviation purposes,” Aviats. Mater. Tekhnol., No. 5, 393–398 (2012).Google Scholar
  5. 5.
    B. S. Lomberg, M. M. Bakradze, E. B. Chabina, and E. V. Filonova, “The relation between the structure and properties of highly heat-resisting nickel alloys for the disks of gas turbine engines,” Aviats. Mater. Tekhnol., No. 2, 25–30 (2011).Google Scholar
  6. 6.
    E. B. Chabina, E. V. Filonova, B. S. Lomberg, and M. M. Bakradze, “The structure of modern deformable nickel alloys,” All Materials: Encyclopedic Handbooh (2012), Vol. 6, pp. 22–27.Google Scholar
  7. 7.
    N. V. Petrushin, E. S. Elyutin, E. B. Chabina, and O. B. Timofeeva, “Phase and structural transitions in heat resistant rhenium-containing alloys of single-crystal structure,” Lit. Proizv., No. 7, 1–7 (2008).Google Scholar
  8. 8.
    N. V. Petrushin, I. L. Svetlov, A. P. Samoilov, et al., “High-temperature phase and structural transitions in single crystals of heat-resistant nickel-alloy, containing rhenium and ruthenium,” Materialovedenie, No. 11, 26–31 (2008).Google Scholar
  9. 9.
    E. N. Kablov, N. V. Petrushin, I. L. Svetlov, and I. H. Demonis, “Nickel lithium heat-resistant alloys of a new generation,” Aviats. Mater. Tekhnol., No. 5, 36–52 (2012).Google Scholar
  10. 10.
    B. S. Lomberg, S. V. Ovsepyan, M. M. Bakradze, and I. S. Mazalov, “High-temperature heat-resistant nickel alloys for the components of gas turbine engines,” ibid., 52–57.Google Scholar
  11. 11.
    B. S. Lomberg, S. V. Ovsepyan, and M. M. Bakradze, “Features of the doping and heat treatment of heat-resistant nickel alloys for the disks of a new generation of gas turbine engines,” Aviats. Mater. Tekhnol., No. 2, 3–8 (2010).Google Scholar
  12. 12.
    B. S. Lomberg, S. V. Ovsepyan, and M. M. Bakradze, “A new heat-resistant nickel alloy for the disks of gas turbine engines and gas turbine equipment,” Materialovedenie, No. 7, 24–28 (2010).Google Scholar
  13. 13.
    J. L. Todoli, L. Gras, V. Hernandis, and J. Mora, “Elemental matrix effects in ICP-AES,” J. Anal. At. Spectrom., No. 17, 142–169 (2002).Google Scholar
  14. 14.
    GOST R ISO12284–2009, Steel and Cast Iron. Selection and Preparation of Samples for Determining the Chemical Composition.Google Scholar
  15. 15.
    GOST 8.563–2009, GSI. Measurement Procedures (Methods).Google Scholar

Copyright information

© Springer Science+Business Media New York 2015

Authors and Affiliations

  • T. N. Zagvozdkina
    • 1
  • F. N. Karachevtsev
    • 1
  • R. M. Dvoretskov
    • 1
  • E. A. Mekhanik
    • 1
  1. 1.State Research Center of the Russian Federation – All-Russia Research Institute of Aviation Materials (VIAM)MoscowRussia

Personalised recommendations