The central analytical laboratory at the ChMK has developed a method of measuring mass fractions of selenium based on atomic-emission and mass-spectrometric analyses. The method is very accurate in measuring low contents of selenium in heat-resistant nickel alloys. The procedure developed for mass-spectrometric analysis of mass fractions of selenium has halved the length of time needed to obtain the analytical results and made the measurement process less labor-intensive.
Similar content being viewed by others
References
GOST 12363–79, Alloy and High-Alloy Steels. Method of Determining Selenium, Izd. Standartov, Moscow (1986).
V. A. Maslov and N. A. Kovaleva, “Determination of selenium micro-impurities in steels and nickel alloys,” in: Proc. 18th Ural Conf. on Spectroscopy, Ekaterinburg (2007), pp. 26–27.
NDP MKh 569–2012, Factory Standard. Measurement Method. Steels and Alloys. Determination of the Mass Fraction of Selenium. Atomic-Emission Method with an Inductively Coupled Argon Plasma, Measurement Method Certificate No. 01.00034/01.1257–2012, Chelyabinsk (2012).
Perkin Elmer SCIEX, ELAN Version 2.4 Software Guide.
A. A. Pupyshev and V. T. Surikov, Mass Spectrometry with an Inductively Coupled Plasma. Formation of Ions [in Russian], UrO RAN, Ekaterinburg (2006).
RMG 76–2004, Federal System for the Standardization of Measurements. Internal Quality Control of the Results of Quantitative Chemical Analyses, Izd. Standartov, Moscow (2006).
Author information
Authors and Affiliations
Corresponding author
Additional information
Translated from Metallurg, No. 4, pp. 82–84, April, 2013.
Rights and permissions
About this article
Cite this article
Maslov, V.A., Tikhonova, V.A., Rafikova, D.G. et al. Method of Measuring the Mass Fraction of Selenium in Heat-Resistant Nickel Alloys. Metallurgist 57, 326–328 (2013). https://doi.org/10.1007/s11015-013-9732-y
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11015-013-9732-y