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Comparative analyses of Roman mortars belonging to different ancient periods from Drobeta-Turnu Severin region

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Abstract

The main object of investigations in this work is the study of the various Roman mortars in Drobeta-Turnu Severin, Romania; the results help clarify the technology used for the construction of the studied sites through different thermoanalytical techniques. The first site encompasses the surviving elements of the Danube Bridge built by the Romans at the beginning of the second century AD to help in their conquest of Dacia. The aim is to establish the extent of similarity or difference between the studied samples. Thermal analysis and infrared spectroscopy are used in the study of different mortar samples. This paper highlights the compatibility of the techniques used: XRD for identifying major crystalline phases, FTIR for a more detailed image for the noncrystalline phase composition and TGA for a quantitative determination of volatile phases (especially CO2 and H2O). The analyses carried out on the mortar samples managed to divide the samples into different categories, obtaining very good correlations between the techniques used. The results also indicate that mortar samples from both the bridge and the Roman Castrum are within known values for Roman mortars.

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References

  1. Vittorio GI. Ponti romani. Catalogo generale, vol. 2. Treviso: Edizioni Canova; 1994.

    Google Scholar 

  2. Griggs FE Jr. Trajan’s bridge: the world’s first long-span wooden bridge. Civil Engineering Practice. 2007;22(1):19–50.

    Google Scholar 

  3. Nemțeanu R. Trajan’s bridge at Drobeta-Turnu Severin built by the architect Apollodorus. ARA Rep. 2011;2:113–26.

    Google Scholar 

  4. Moşoiu C, Vlase D, Vlase G, Lazău R, Vlase T. TG-DTA and FTIR analyses of roman and later historic mortars from Drobeta-Turnu Severin region. J Therm Anal Calorim. 2019;138(3):2159–66.

    Article  Google Scholar 

  5. Silva DA, Wenk HR, Monteiro PJM. Comparative investigation of mortars from Roman Colosseum and cistern. Thermochim Acta. 2005;438:35–40.

    Article  CAS  Google Scholar 

  6. Duran A, Perez-Maqueda L, Poyato J, Perez-Maqueda J. A thermal study approach to roman age wall painting mortars. J Therm Anal Calorim. 2010;99:803–9.

    Article  CAS  Google Scholar 

  7. Vecchio S, La Gmestra A, Frezza A, Ferragina C. The use of thermoanalytical techniques in the characterization of ancient mortars. Thermochim Acta. 1993;227:215–23.

    Article  CAS  Google Scholar 

  8. Biscontin G, Pellizon Birelli M, Zendri E. Characterisation of binders employed in the manufacture of Venetian historical mortars. J Cult Herit. 2000;3:31–7.

    Article  Google Scholar 

  9. Anastasiou M, Hasapis T, Zorba T, Pavlidou E, Chrissafis K, Paraskevopoulos KM. TG-DTA and FTIE analyses of plasters from byzantine monuments in Balkan region-comparative study. J Therm Anal Calorim. 2006;84:27–32.

    Article  CAS  Google Scholar 

  10. Catauro M, Bollino F, Dell’Era A, Ciprioti SV. Pure Al2O3· 2SiO2 synthesized via a sol-gel technique as a raw material to replace metakaolin: chemical and structural characterization and thermal behavior. Ceram Int. 2016;42(14):16303–9.

    Article  CAS  Google Scholar 

  11. Catauro M, Papale F, Lamanna G, Bollino F. Geopolymer/PEG hybrid materials synthesis and investigation of the polymer influence on microstructure and mechanical behavior. Mater Res. 2015;18:698–705.

    Article  CAS  Google Scholar 

  12. Dambrauskas T, Baltakys K, Eisinas A. Formation and thermal stability of calcium silicate hydrate substituted with Al3+ ions in the mixtures with CaO/SiO2 = 1.5. J Therm Anal Calorim. 2018;131:501–12.

    Article  CAS  Google Scholar 

  13. Kani EN, Allahverdi A, Provis JL. Calorimetric study of geopolymer binders based on natural Pozzolan. J Therm Anal Calorim. 2017;127:2181–90.

    Article  Google Scholar 

  14. Zhi Z, Ma B, Jian S, Guo Y, Yu H, Tan H, Chen F. Thermal analyses. Effect of cellulose ethers on hydration of high-strength gypsum. J Therm Anal Calorim. 2017;129:1547–54.

    Article  CAS  Google Scholar 

  15. Scheinherrova L, Dolezelova M, Havlın J, Trnık A. Thermal analysis of ternary gypsum-based binders stored in different environments. J Therm Anal Calorim. 2018;133:177–88.

    Article  CAS  Google Scholar 

  16. Bakolas A, Biscontin G, Moropouloub A, Zendri E. Characterization of structural byzantine mortars by thermogravimetric analysis. Thermochim Acta. 1998;321:151–60.

    Article  CAS  Google Scholar 

  17. Gaviria X, Borrachero MV, Paya J, Monzo JM, Tobon JI. Mineralogical evolution of cement pastes at early ages based on thermogravimetric analysis (TG). J Therm Anal Calorim. 2018;132:39–46.

    Article  CAS  Google Scholar 

  18. Vlase D, Rogozea O, Moşoiu C, Vlase G, Lazău R, Vlase T. Thermoanalytical investigations of some ceramics dated from the Neolithic period, discovered at Oxenbrickel, Sânandrei, Romania. J Therm Anal Calorim. 2019;138:2145–57.

    Article  CAS  Google Scholar 

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Acknowledgements

We would like to thank archaeologists Marin Neagoe, PhD, and Oana Neagoe, PhD, from Museum of the Iron Gates Region, for providing the samples.

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Authors and Affiliations

  1. Research Centre for Thermal Analysis in Environmental Problems, West University of Timisoara, Pestalozzi Street 16, Timisoara, Romania

    Dan Vlase, Moşoiu Codruţa, Gabriela Vlase & Titus Vlase

  2. Department of Scientific Research and Academic Creation, West University of Timisoara, Parvan Bvd. 4, Timisoara, Romania

    Dan Vlase

  3. Faculty of Industrial Chemistry and Environmental Engineering, Politehnica University Timisoara, Victoriei Square 2, 300006, Timisoara, Romania

    Radu Lazău

Authors
  1. Dan Vlase
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  2. Moşoiu Codruţa
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  3. Gabriela Vlase
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  4. Radu Lazău
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  5. Titus Vlase
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Correspondence to Gabriela Vlase or Radu Lazău.

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Vlase, D., Codruţa, M., Vlase, G. et al. Comparative analyses of Roman mortars belonging to different ancient periods from Drobeta-Turnu Severin region. J Therm Anal Calorim 141, 991–998 (2020). https://doi.org/10.1007/s10973-020-09917-z

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  • DOI: https://doi.org/10.1007/s10973-020-09917-z

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