In this paper was assessed the influence of carbon black (CB) powder on the hydration and hardening processes of Portland cement (PC)-based materials; this type of materials is designed to be used as cement-based sensors in structural or pavement health monitoring. The rate of PC hydration and hardening processes is influenced by the amount of CB addition, with direct consequences on some properties of these materials, i.e., water for normal consistency and setting time. These results coupled with those obtained by thermal and X-ray diffraction analyses suggest a delaying effect of PC hydration and hardening processes in the presence of carbon black powder, most likely as a result of CB nanoparticles high adsorbent surface. Compressive strength values of PC mortars with CB content up to 1 mass%, assessed after 28 days of hardening, are comparable with those of PC mortars; thus, these materials can be successfully used in construction.
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Monteiro AO, Cachim PB, Costa PMFJ. Self-sensing piezoresistive cement composite loaded with carbon black particles. Cem Concr Compos. 2017;81:59–65.
Alavi AH, Hasni H, Lajnef N, Chatti K. Continuous health monitoring of pavement systems using smart sensing technology. Constr Build Mater. 2016;114:719–36.
Zhu S, Chung DDL. Analytical model of piezoresistivity for strain sensing in carbon fiber polymer–matrix structural composite under flexure. Carbon. 2007;45(8):1606–13.
Ding Y, Chen ZI, Han Z, Zhang Y, Pacheco-Torgal F. Nano-carbon black and carbon fiber as conductive materials for the diagnosing of the damage of concrete beam. Constr Build Mater. 2013;43:233–41.
Chung DDL. Piezoresistive cement-based materials for strain sensing. J Intell Mater Syst Struct. 2002;13(9):599–609.
Boris R, Antonovic V, Keriene J, Stonys R. The effect of carbon fiber additive on early hydration of calcium aluminate cement. J Therm Anal Calorim. 2016;125(3):1061–70.
Al-Dahawi A, Öztürk O, Emami F, Yıldırım G, Şahmaran M. Effect of mixing methods on the electrical properties of cementitious composites incorporating different carbon-based materials. Constr Build Mater. 2016;104:160–8.
Al-Dahawi A, Sarwary MH, Öztürk O, Yıldırım G, Akın A, Şahmaran M, Lachem M. Electrical percolation threshold of cementitious composites possessing self-sensing functionality incorporating different carbon-based materials. Smart Mater Struct. 2016;25:105005.
Al-Dahawi A, Yıldırım G, Öztürk O, Şahmaran M. Assessment of self-sensing capability of engineered cementitious composites within the elastic and plastic ranges of cyclic flexural loading. Constr Build Mater. 2017;145:1–10.
Siad H, Lachemi M, Sahmaran M, Mesbah HA, Hossain KA. Advanced engineered cementitious composites with combined self-sensing and self-healing functionalities. Constr Build Mater. 2018;176:313–22.
Yıldırım G, Sarwary MH, Al-Dahawi A, Öztürk O, Anıl O, Şahmaran M. Piezoresistive behavior of CF- and CNT-based reinforced concrete beams subjected to static flexural loading: Shear failure investigation. Constr Build Mater. 2018;168:266–79.
D’Alessandro A, Rallini M, Ubertini F, Materazzi AL, Kenny JM. Investigations on scalable fabrication procedures for self-sensing carbon nanotube cement-matrix composites for SHM applications. Cem Concr Compos. 2016;65:200–13.
Konsta-Gdoutos MS, Aza CA. Self sensing carbon nanotube (CNT) and nanofiber (CNF) cementitious composites for real time damage assessment in smart structures. Cem Concr Compos. 2014;53:162–9.
Sun MQ, Liew RJY, Zhang MH, Li W. Development of cement-based strain sensor for health monitoring of ultra high strength concrete. Constr Build Mater. 2014;65:630–7.
Parveen S, Rana S, Fangueiro R, Paiva MC. Microstructure and mechanical properties of carbon nanotube reinforced cementitious composites developed using a novel dispersion technique. Cem Concr Res. 2015;73:215–27.
Teomete E, Kocyigit OI. Tensile strain sensitivity of steel fiber reinforced cement matrix composites tested by split tensile test. Constr Build Mater. 2013;47:962–8.
Shi L, Lu Y, Bai Y. Mechanical and electrical characterisation of steel fiber and carbon black engineered cementitious composites. Procedia Eng. 2017;188:325–32.
Monteiro AO, Cachim PB, Costa PMFJ. Electrical properties of cement-based composites containing carbon black particles. Mater Today Proc. 2015;2(1):193–9.
Monteiro AO, Loredo A, Costa PMFJ, Oeser M, Cachim PB. A pressure-sensitive carbon black cement composite for traffic monitoring. Constr Build Mater. 2017;154:1079–86.
Han B, Yu X, Ou J. Self-sensing concrete in smart structures. Oxford: Butterworth Heinemann; 2014.
Han B, Ding S, Yu X. Intrinsic self-sensing concrete and structures: a review. Measurement. 2015;59:110–28.
Dambrauskas T, Baltakys K, Skamat J, Kudzma A. Hydration peculiarities of high basicity calcium silicate hydrate samples. J Therm Anal Calorim. 2018;131(1):491–9.
Bhattacharya M, Harish KV. An integrated approach for studying the hydration of Portland cement systems containing silica fume. Constr Build Mater. 2018;188:1179–92.
Dambrauskas T, Baltakys K, Eisinas A. Formation and thermal stability of calcium silicate hydrate substituted with Al3+ ions in the mixtures with CaO/SiO2 = 1.5. J Therm Anal Calorim. 2018;131(1):501–12.
Trauchessec R, Mechling JM, Lecomte A, Roux A, Le Rolland B. Hydration of ordinary Portland cement and calcium sulfoaluminate cement blends. Cem Concr Compos. 2015;56:106–14.
Maciel MH, Soares GS, Romano RCO, Cincotto MA. Monitoring of Portland cement chemical reaction and quantification of the hydrated products by XRD and TG in function of the stoppage hydration technique. J Therm Anal Calorim. 2018. https://doi.org/10.1007/s10973-018-7734-5.
Romano RCO, Bernardo HM, Maciel MH, Pileggi RG, Cincotto MA. Hydration of Portland cement with red mud as mineral addition. J Therm Anal Calorim. 2018;131(3):2477–90.
Zhang J, Li G, Ye W, Chang Y, Liu Q, Song Z. Effects of ordinary Portland cement on the early properties and hydration of calcium sulfoaluminate cement. Constr Build Mater. 2018;186:1144–53.
El-Gamal SMA, Abo-El-Enein SA, El-Hosiny FI, Amin MS, Ramadan M. Thermal resistance, microstructure and mechanical properties of type I Portland cement pastes containing low-cost nanoparticles. J Therm Anal Calorim. 2018;131(2):949–68.
SR EN 196–3. Methods of testing cement—Part 3: determination of setting time and soundness. 2017.
SR EN 196–1. Methods of testing cement - Part 1: Determination of strength. 2016.
Neville AM. Properties of concrete. 4th ed. London: Longman; 1998.
Badanoiu A, Paceagiu J, Voicu G. Hydration and hardening processes of Portland cements obtained from clinkers mineralized with fluoride and oxides. J Therm Anal Calorim. 2011;103(3):879–88.
Campbell DH. Microscopical examination and interpretation of Portland cement and clinker. 2nd ed. Skokie: Portland Cement Association; 1999.
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Pârvan, MG., Voicu, G. & Bădănoiu, AI. Study of hydration and hardening processes of self-sensing cement-based materials with carbon black content. J Therm Anal Calorim 139, 807–815 (2020). https://doi.org/10.1007/s10973-019-08535-8
- Carbon black
- Hydration processes
- Thermal analysis