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Journal of Sol-Gel Science and Technology

, Volume 81, Issue 2, pp 436–441 | Cite as

A facile synthesis for magnetic ferberite nanostructured material

Original Paper: Nano-structured materials (particles, fibers, colloids, composites, etc.)

Abstract

Iron-tungsten oxide nanospinel have been prepared by two methods: microwave combustion method and Pechini method. The W-Fe bimetallic ferberite was successfully synthesized by microwave-assisted techniques. The resultant magnetic nanocomposites were characterized by thermal analysis, X-ray diffraction, Fourier transform infrared spectroscopy, Raman spectroscopy, energy-dispersive X-ray, transmission electron microscopy, nitrogen adsorption, and magnetic properties measurement system. The prepared ferberite nanoparticles (50–65 nm) using microwave combustion method were pure monoclinic ferberite. The ferberite nanoparticles showed ferrimagnetic hysteresis loop with values of saturation magnetization and coercivity of 4.829 A.m2/Kg and 0.0312 T, successively.

Graphical Abstract

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Keywords

Magnetic ferberite Microwave-assisted synthesis Wolframite structure Pechini synthesis FeWO4 

Notes

Compliance with ethical standards

Conflict of interest

The authors declare that they have no conflict of interest.

Supplementary material

10971_2016_4195_MOESM1_ESM.doc (146 kb)
Supplementary Information

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Copyright information

© Springer Science+Business Media New York 2016

Authors and Affiliations

  1. 1.Catalysis Department, Refining DivisionEgyptian Petroleum Research InstituteCairoEgypt
  2. 2.EPRI Nanotechnology CenterEgyptian Petroleum Research InstituteCairoEgypt

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