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Journal of Radioanalytical and Nuclear Chemistry

, Volume 310, Issue 1, pp 99–108 | Cite as

A dispersive liquid–liquid microextraction technique for the determination of 210Pb in drinking water samples

  • Baki B. Sadi
  • Jae Y. Lee
  • Jing Chen
Article

Abstract

A radioanalytical method has been developed for determination of 210Pb in drinking water samples. It is based on the conversion of inorganic lead into tetraethyl lead using an alkylating reagent followed by a dispersive liquid–liquid microextraction of tetraethyl lead to toluene. Method performance for selectivity, interference, minimum detectable activity, minimum quantifiable concentration, relative error, and relative standard deviation is considered to be satisfactory for determination of 210Pb in drinking water for radiological protection. The method presented here offers a significant improvement in sample turnaround time (<7 h) compared to the existing analytical methods that take 2–6 days.

Keywords

210Pb Radioactivity Internal contamination 

Supplementary material

10967_2016_4833_MOESM1_ESM.docx (131 kb)
Supplementary material 1 (DOCX 130 kb)

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Copyright information

© Akadémiai Kiadó, Budapest, Hungary 2016

Authors and Affiliations

  1. 1.Radiation Protection BureauHealth CanadaOttawaCanada

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