Advertisement

Journal of Radioanalytical and Nuclear Chemistry

, Volume 278, Issue 3, pp 789–794 | Cite as

Micro-PIXE characterization of reference samples intended for QA/QC of k0 NAA

  • T. Bučar
  • B. Smodiš
  • P. Pelicon
  • J. Simčič
  • R. Jaćimović
QA/QC

Abstract

Cellulose cylinders and circular filter papers spiked with known amounts of standard element solutions were prepared for studying some aspects of assessing measurement uncertainty of NAA and the elemental distribution measured by micro-PIXE analysis. Results for the cylinders showed strongly non-homogeneous distribution of the elements, both in radial and vertical directions, dominantly caused by osmosis driven transport of added liquid solution from the centre to the edges. Results for the thin cellulose filter paper disks exhibited weaker peaking of the standard element concentrations at the edges in comparison with the thick cylinders.

Keywords

Neutron Activation Analysis PIXE Nitric Acid Solution Reference Element Proton Flux 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    B. Smodiš, Vestn. Slov. Kem. Drus., 39 (1992) 503.Google Scholar
  2. 2.
    F. De Corte, R. Van Sluijs, A. Simonits, J. Kučera, B. Smodiš, A. R. Byrne, A. De Wispelaere, D. Bossus, J. Frána, Z. Horák, R. Jaćimović, Appl. Radiation Isotopes, 55 (2001) 347.CrossRefGoogle Scholar
  3. 3.
    R. Jaćimović, B. Smodiš, T. Bučar, P. Stegnar, J. Radioanal. Nucl. Chem., 257 (2003) 659.CrossRefGoogle Scholar
  4. 4.
    B. Smodiš, T. Bučar, J. Radioanal. Nucl. Chem., 269 (2006) 311.CrossRefGoogle Scholar
  5. 5.
    T. Bučar, B. Smodiš, Nucl. Instr. Meth., A564 (2006) 683.Google Scholar
  6. 6.
    R. Zeissler, R. M. Lindstrom, R. R. Greenberg, J. Radioanal. Nucl. Chem., 263 (2005) 315.Google Scholar
  7. 7.
    J. Simčič, P. Pelicon, M. Budnar, Ž. Šmit, Nucl. Instr. Meth., B190 (2002) 283.Google Scholar
  8. 8.
    J. L. Campbell, T. L. Hopman, J. A. Maxwell, Z. Nejedly, Nucl. Instr. Meth., B170 (2000) 193.Google Scholar

Copyright information

© Springer Science+Business Media, LLC. 2008

Authors and Affiliations

  • T. Bučar
    • 1
  • B. Smodiš
    • 1
  • P. Pelicon
    • 1
  • J. Simčič
    • 1
  • R. Jaćimović
    • 1
  1. 1.Jožef Stefan InstituteLjubljanaSlovenia

Personalised recommendations