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Journal of Structural Chemistry

, Volume 51, Issue 4, pp 765–768 | Cite as

Crystal Structure of A Molecular Complex Compound of Antimony(III) Fluoride with L-Leucine

  • A. A. Udovenko
  • N. V. Makarenko
  • R. L. Davidovich
  • L. A. Zemnukhova
  • E. V. Kovaleva
Article

Abstract

Single crystal X-ray diffraction analysis is used to determine the crystal structure of a newly synthesized molecular complex compound of antimony(III) fluoride with L-leucine of the composition SbF3(C6H13NO2) (orthohombic crystal system: a = 5.7948(8) Å, b = 6.2433(9) Å, c = 28.594(4) Å, Z = 4, P212121 space group). The structure consists of SbF3 molecules and L-leucine bound into polymer chains by bidentate bridging carboxyl groups of amino acid molecules. Weak Sb…F(1)b bonds combine the adjacent chains into polymer ribbons organized by N-H…. F and N-H…. O hydrogen bonds into a framework.

Key words

single crystal X-ray diffraction analysis crystal structure antimony(III) fluoride L-leucine molecular complex compound 

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Copyright information

© Pleiades Publishing, Ltd. 2010

Authors and Affiliations

  • A. A. Udovenko
    • 1
  • N. V. Makarenko
    • 1
  • R. L. Davidovich
    • 1
  • L. A. Zemnukhova
    • 1
  • E. V. Kovaleva
    • 1
  1. 1.Institute of Chemistry, Far East DivisionRussian Academy of SciencesVladivostokRussia

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