Journal of Porous Materials

, Volume 18, Issue 4, pp 435–441 | Cite as

Porous TiO2 nanostructures synthesized from peroxotitanic acid-derived anatase

  • W. Q. Peng
  • Y.-J. Liu
  • M. Aizawa
  • Z.-M. Wang
  • H. Hatori
  • T. Hirotsu


Titania/titanate nanotubes and nanoplates were prepared by an alkali hydrothermal method using the powder and the sol of peroxotitanic acid-derived anatase, respectively, as precursors. XRD patterns and Raman spectra showed that both nanotubes and nanoplates are of titanate structure with the latter involving a slight part of anatase phase. These nanotubes and nanoplates are highly mesoporous based on nitrogen adsorption measurement. After calcination at 823 K, nanotubes were transformed into nanorods, and nanoplates into spherical particles, both of which are pure anatase-type titania. The nanorod material exhibits an enhanced photocatalytic activity in comparison with the spherical particles.

Graphical Abstract

FE-SEM images of nanotubes (left) and nanoplates (right) prepared using the powder and the sol of peroxotitanic acid-derived anatase as precursors, respectively.


Nanostructures TiO2 Precursors Photocatalysis 


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Copyright information

© Springer Science+Business Media, LLC 2010

Authors and Affiliations

  1. 1.Energy Technology Research InstituteNational Institute of Advanced Industrial Science and TechnologyTsukubaJapan
  2. 2.Health Technology Research CenterNational Institute of Advanced Industrial Science and TechnologyTakamatsu-shiJapan

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