Advertisement

Sonochemical Synthesis of a New Lead(II) Coordination Polymer with 2-Quinoline Carboxylate Ligand: A Precursor for the Preparation of Nano-structured Lead(II) Oxide

  • Akram Panjehpour
  • Ali Morsali
Article

Abstract

Crystalline and nano-structure of a new Pb(II) coordination polymer, [Pb(NO2)(2-quc)]n (1), {Hquc = 2-quinoline carboxylic acid} is synthesized via heat gradient and sonochemical methods, respectively. The newly synthesized structures are characterized by scanning electron microscopy (SEM), X- ray powder diffraction (XRD), IR and 1HNMR spectroscopies, elemental analyses and single crystal X-ray diffraction is used to understand the exact structure of the crystalline 1. Thermal stability of nano and bulk samples of compound 1 are studied and compared through thermal gravimetric and differential thermal analyses. PbO nanoparticles are then produced by calcination of the nano-structure of compound 1 at 600 °C. The obtained PbO is characterized by XRD and SEM analyses.

Keywords

Nano-structure Coordination polymer Lead(II) PbO Crystal structure 

Notes

Acknowledgments

This work is financially supported by Payame Noor and Tarbiat Modares universities.

References

  1. 1.
    L. Hashemi, A. Morsali, Cryst. Eng. Commun. 14, 779 (2012)Google Scholar
  2. 2.
    S. Noro, S. kitagawa, T.A. kutagawa, T. Nakamura, Prog. Polym. Sci. 34, 240 (2009)CrossRefGoogle Scholar
  3. 3.
    F. Jing Liu, D. Sun, H. Jun Hao, R.B. Huang, L.S. Zheng, Cryst. Growth Des. 12, 354 (2012)CrossRefGoogle Scholar
  4. 4.
    A. Erxleben, Coord. Chem. Rev. 246, 203 (2003)CrossRefGoogle Scholar
  5. 5.
    A. Morsali, M.Y. Masoumi, Coord. Chem. Rev. 253, 1882 (2009)CrossRefGoogle Scholar
  6. 6.
    K.-T.Wong, J.-M. LEHN, S.-M. Peng, G.-H. Lee, Chem. Commun. (2000) 2259. doi: 10.1039/B005679K
  7. 7.
    A.G. Bunn, P.J. Carroll, B.B. Wayland, Inorg. Chem. 31, 1297 (1992)CrossRefGoogle Scholar
  8. 8.
    M.A.M. Abu-Youssef, A. Escuer, D. Gatteschi, M.A.S. Goher, F.A. Mautner, R. Vicente, Inorg. Chem. 38, 5716 (1999)CrossRefGoogle Scholar
  9. 9.
    M. Aoyagi, K. Biradha, M. Fujita, J. Am. Chem. Soc. 121, 7457 (1999)CrossRefGoogle Scholar
  10. 10.
    M. Fujita, Y.J. Kwon, S. Washizu, K.J. Ogura, J. Am. Chem. Soc. 116, 1151 (1994)CrossRefGoogle Scholar
  11. 11.
    D.S. Chowdhuri, A. Rana, M. Bera, E. Zangrando, S. Dalai, Polyhedron 28, 2131 (2009)CrossRefGoogle Scholar
  12. 12.
    R.L. Davidovich, V. Stavila, D.V. Marinin, E.I. Voit, K.H. Whitmire, Coord. Chem. Rev. 253, 1316 (2009)CrossRefGoogle Scholar
  13. 13.
    A. Morsali, J. Abedini, Inorg. Chem. Commun. 8, 460 (2005)CrossRefGoogle Scholar
  14. 14.
    A.A. Soudi, F. Marandi, A. Ramazani, E. Ahmadi, A. Morsali, C. R. Chimie 8, 157 (2005)CrossRefGoogle Scholar
  15. 15.
    U. Englert, Coord. Chem. Rev. 254, 537 (2010)CrossRefGoogle Scholar
  16. 16.
    A. Morsali, A.R. Mahjoub, M.J. Soltanian, S.J. Darzi, Z. Anorg. Allg. Chem. 629, 2596 (2003)CrossRefGoogle Scholar
  17. 17.
    A. Morsali, A.R. Mahjoub, J. Chem. Coord. 56, 779 (2003)CrossRefGoogle Scholar
  18. 18.
    W.-J. Shi, L. Hou, D. Li, Y.-G. Yin, Inorg. Chim. Acta 360, 588 (2007)CrossRefGoogle Scholar
  19. 19.
    A. Morsali, H.H. Monfared, A. Morsli, Inorg. Chim. Acta 362, 3427 (2009)CrossRefGoogle Scholar
  20. 20.
    N. Le Narvor, L. Toupet, C.L. Apinte, J. Am. Chem. Soc. 117, 7129 (1995)CrossRefGoogle Scholar
  21. 21.
    A. Caneschi, D. Gatteschi, N. Lalioti, C. Sangregorio, R. Sessoli, G. Venturi, A. Vindigni, A. Rettori, M.G. Pini, M.A. Novak, Angew. Chem. Int. Ed. 40, 1760 (2001)CrossRefGoogle Scholar
  22. 22.
    J. Parr, Polyhedron 16, 551 (1997)CrossRefGoogle Scholar
  23. 23.
    J.M. Harrowfield, H. Miyamae, B.W. Skelton, A.A. Soudi, A.H. White, Aust. J. Chem. 49, 1029 (1996)CrossRefGoogle Scholar
  24. 24.
    Z. Wang, Q. Wei, G. Xie, Q. Yang, S. Chen, S. Gao, J. Coord. Chem. 65, 286 (2012)CrossRefGoogle Scholar
  25. 25.
    J.C. Bailar Jr, Prep. Inorg. React. 1, 1 (1964)Google Scholar
  26. 26.
    A.R. Abbasi, M. Bohloulzadeh, A. Morsali, J. Inorg. Organomet. Polym. (2011). doi: 10.1007/s10904-011-9484-8
  27. 27.
    A.R. Abbasi, A. Morsali, Ultrason. Sonochem. 17, 704 (2010)CrossRefGoogle Scholar
  28. 28.
    A.R. Abbasi, A. Morsali, Ultrason. Sonochem. 18, 282 (2011)CrossRefGoogle Scholar
  29. 29.
    V. Safarifard, A. Morsali, Ultrason. Sonochem. 19, 300 (2012)CrossRefGoogle Scholar
  30. 30.
    A.R. Abbasi, H. Kalantary, M. Yousefi, A. Ramazani, A. Morsali, Ultrason. Sonochem. (2012). doi: 10.1016/J.ULTSONCH.2011.11.011 Google Scholar
  31. 31.
    L. Aboutorabi, A. Morsali, Inorg. Chimi. Acta. 363, 2506 (2010)CrossRefGoogle Scholar
  32. 32.
    A. Aslani, A. Morsali, V.T. Yilmaz, C. Kazak, J. Mol. Struct. 929, 187 (2009)CrossRefGoogle Scholar
  33. 33.
    L. Hashemi, A. Morsali, J. Neurosurg. 1, 89 (2012)Google Scholar
  34. 34.
    Y. Hanifehpour, B. Mirtamizdoust, S.W. Joo, J. Inorg. Organomet. polym. (2012). doi: 10.1007/s10904-012-9654-3
  35. 35.
    V. Safarifard, A. Morsali, ultrasonic Sonochem. (2012). doi: 10.1016/j.ultsonch.2011.12.013
  36. 36.
    L. Hashemi, A. Morsali, P. Retailleau, Inorg. Chimi. Acta. 367, 207 (2011)CrossRefGoogle Scholar
  37. 37.
    H. Sadeghzadeh, A. Morsali, P. Retailleau, Polyhedron 29, 925 (2010)CrossRefGoogle Scholar
  38. 38.
    M. Sugimoto, J. Magn, Chem. Mater. 133, 460 (1994)Google Scholar
  39. 39.
    T. Ding, J.J. zhu, J.M. Hong, Mater. Lett. 57, 4445 (2003)CrossRefGoogle Scholar
  40. 40.
    A.R. Abbasi, A. Morsali, Ultrason. Sonochem. 17, 572 (2010)CrossRefGoogle Scholar
  41. 41.
    M.V. Landau, L. Vradman, M. Herskowitz, Y. Koltypin, J. Catal. 201, 22 (2001)CrossRefGoogle Scholar
  42. 42.
    H. Wang, Y.N. Lu, J.J. Zhu, H.Y. Chem, Inorg. Chem. 42, 6404 (2003)CrossRefGoogle Scholar
  43. 43.
    J.H. Zhang, Z. chen, Z.L. Wang, N.B. Ming, J. Mater. Res. 18, 1804 (2003)CrossRefGoogle Scholar
  44. 44.
    F. Marandi, V. Safarifard, A, Morsali, H. Kun Fun. J. Coord. Chem. 64, 3781 (2011)CrossRefGoogle Scholar
  45. 45.
    K.S. Suslick, S.B. Choe, A.A. Cichowlas, M.W. Grinstaff, Nature 353, 414 (1991)CrossRefGoogle Scholar
  46. 46.
    A. Ramazani, S. Hamidi, A. Morsali, J. Mol. Liq. 157, 73 (2010)CrossRefGoogle Scholar
  47. 47.
    Z. Rashidi, A. Morsali, Polyhedron 30, 929 (2011)CrossRefGoogle Scholar
  48. 48.
    H. Haddadian, A.R. Aslani, A. Morsali, Inorg. Chimi. Acta. 362, 1805 (2009)CrossRefGoogle Scholar
  49. 49.
    H. Sadeghzadeh, A. Morsali, V.T. Yilmaz, O. Buyukgungor, Ultrason. Sonochem. 17, 592 (2010)CrossRefGoogle Scholar
  50. 50.
    W.Z. Zhang, D.Z. Wei, E.J. Gao, Y.G. Sun, J. Struct. Chem. 26, 357 (2007)Google Scholar
  51. 51.
    E. Najafi, M.M. Amini, S.W. Ng, Acta Crystallogr. 67, 264 (2011)CrossRefGoogle Scholar
  52. 52.
    G. Mohammadnezhad, A.R. Ghanbarpour, M.M. Amini, S.W. Ng, Acta Crystallogr. 66, 963 (2010)Google Scholar
  53. 53.
    M. Martos, J. Morales, L. Sanchez, R. Ayouchi, D. leinen, F. Martin, J.R. Ramos, Electrochim. Acta 45, 2939 (2001)CrossRefGoogle Scholar
  54. 54.
    M. Cao, Y. Meng, Y. Lu, Catal. Commun. 6, 802 (2005)CrossRefGoogle Scholar
  55. 55.
    L. Amarande, C. Miclea, C. Tanasoiu, J. Euro, Ceram. Soc. 22, 1269 (2002)CrossRefGoogle Scholar
  56. 56.
    A.V. Murugan, R.S. Sonawane, B.B. Kale, S.K. Apte, A.V. Kulkami, Mater. Chem. Phys. 71, 98 (2001)CrossRefGoogle Scholar
  57. 57.
    S.H. Ysu, J. Yang, Z.H. Han, Y. Zhou, R.Y. Yang, Y.T. Qian, Y.H. Zhanga, J. Mater. Chem. 9, 1283 (1999)CrossRefGoogle Scholar
  58. 58.
    X. Yarg, B. Yarg, Y. Yan, Y.T. Qian, J. Cryst. Growth 291, 45 (2006)CrossRefGoogle Scholar
  59. 59.
    J. Yang, J.H. Zeng, S.H. Yu, L. Yang, G.E. Zhou, Y.T. Qian, Chem. Mater. 12, 3259 (2000)CrossRefGoogle Scholar
  60. 60.
    Mercury 1.4.1, Copyright (Cambridge Crystallographic Data, Cambridge, 2001)Google Scholar
  61. 61.
    K. Nakamoto, Infrared and Raman Spectra of inorganic and coordination compounds, 5th edn. (Wiley, New York, 1997)Google Scholar
  62. 62.
    L. Shimoni-Livny, J.P. Glusker, C.W. Bock, Inorg. Chem. 37, 1853 (1998)CrossRefGoogle Scholar
  63. 63.
    H. Ahmadzadi, F. Marandi, A. Morsali, J. Inorg. Organomet. Polym. 694, 3565 (2009)Google Scholar
  64. 64.
    A.R. Aslani, A. Morsali, Inorg. Chimi. Acta. 362, 5012 (2009)CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC 2012

Authors and Affiliations

  1. 1.Department of ChemistryPayame Noor UniversityTehranIslamic Republic of Iran
  2. 2.Department of Chemistry, Faculty of SciencesTarbiat Modares UniversityTehranIslamic Republic of Iran

Personalised recommendations